dimethyl-bis(4-nitrophenyl)stannane

Base Information

Chemical Name:dimethyl-bis(4-nitrophenyl)stannane
CAS No.:910327-35-4
Molecular Formula:C₁₄H₁₄N₂O₄Sn
Molecular Weight:392.986
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dimethyl-bis(4-nitrophenyl)stannane

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Technology Process of dimethyl-bis(4-nitrophenyl)stannane

There total 1 articles about dimethyl-bis(4-nitrophenyl)stannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: 7616-94-6
perchloryl fluoride

: 52323-94-1
trimethyl(4-nitrophenyl)stannane

: trimethyltin fluoride

: 910327-35-4
dimethyl-bis(4-nitrophenyl)stannane

Guidance literature:: In tetrahydrofuran; byproducts: nitrobenzene; trimethyl-(4-nitrophenyl)stannane dissolved in dry THF was cooled at -60°C; FClO3/N2 mixt. passed through soln. for about 35 min; soln. warmed up to ambient temp. under stirring and stirred at about 60°C for 20 min (closed conditions); isolated by semi-preparative thin-layer chromy. (silica gel 60, petroleum ether/ethyl acetate 10:1); elem. anal.;
DOI:10.1016/j.jorganchem.2006.04.023