PdBr₂((C₆H₅)2P(CH₂)2P(C₆H₅)2CHC(O)C₆H₅)

Base Information

Chemical Name:PdBr₂((C₆H₅)2P(CH₂)2P(C₆H₅)2CHC(O)C₆H₅)
CAS No.:58628-90-3
Molecular Formula:C₃₄H₃₀Br₂OP₂Pd
Molecular Weight:782.787
Hs Code.:

PdBr<sub>2</sub>((C<sub>6</sub>H<sub>5</sub>)2P(CH<sub>2</sub>)2P(C<sub>6</sub>H<sub>5</sub>)2CHC(O)C<sub>6</sub>H<sub>5</sub>)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of PdBr₂((C₆H₅)2P(CH₂)2P(C₆H₅)2CHC(O)C₆H₅)

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Technology Process of PdBr₂((C₆H₅)2P(CH₂)2P(C₆H₅)2CHC(O)C₆H₅)

There total 1 articles about PdBr₂((C₆H₅)2P(CH₂)2P(C₆H₅)2CHC(O)C₆H₅) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14220-64-5,39958-10-6,15617-18-2
bis(benzonitrile)palladium(II) chloride

: 55343-39-0
((C₆H₅)2P(CH₂)2P(C₆H₅)2CH₂C(O)C₆H₅)⁽¹⁺⁾*Br^(1-)=((C₆H₅)2P(CH₂)2P(C₆H₅)2CH₂C(O)C₆H₅)Br

: 7647-15-6
sodium bromide

: 58628-90-3
PdBr₂((C₆H₅)2P(CH₂)2P(C₆H₅)2CHC(O)C₆H₅)

Guidance literature:: With KOH; catalyst: 18-crown-6; In potassium hydroxide; dichloromethane; aq. KOH; addn. of Pd-complex to a soln. of P-ylide in CH2Cl2, followed by aq. KOH and 18-crown-6, stirring for 30 min, addn. of NaBr in MeOH, reaction is continued for 30 min; addn. of H2O and CH2Cl2, sepn. of the org. layer, washing with H2O (three times), drying (with MgSO4), filtn., evapn. to dryness (vac. evaporator), washing with Et2O, recrystn. from CH3Cl/n-hexane, elem. anal.;
DOI:10.1039/DT9900002509