(3aR)-1t-((S)-1,5-dimethyl-hexyl)-4t-(3,5-dinitro-benzoyloxy)-7a-methyl-(3ar,7at)-hexahydro-indan

Base Information

Chemical Name:(3aR)-1t-((S)-1,5-dimethyl-hexyl)-4t-(3,5-dinitro-benzoyloxy)-7a-methyl-(3ar,7at)-hexahydro-indan
CAS No.:119569-20-9
Molecular Formula:C₂₅H₃₆N₂O₆
Molecular Weight:460.571
Hs Code.:

(3a<i>R</i>)-1<i>t</i>-((<i>S</i>)-1,5-dimethyl-hexyl)-4<i>t</i>-(3,5-dinitro-benzoyloxy)-7a-methyl-(3a<i>r</i>,7a<i>t</i>)-hexahydro-indan

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3aR)-1t-((S)-1,5-dimethyl-hexyl)-4t-(3,5-dinitro-benzoyloxy)-7a-methyl-(3ar,7at)-hexahydro-indan

Chemical Property:

Purity/Quality:

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Technology Process of (3aR)-1t-((S)-1,5-dimethyl-hexyl)-4t-(3,5-dinitro-benzoyloxy)-7a-methyl-(3ar,7at)-hexahydro-indan

There total 12 articles about (3aR)-1t-((S)-1,5-dimethyl-hexyl)-4t-(3,5-dinitro-benzoyloxy)-7a-methyl-(3ar,7at)-hexahydro-indan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 199798-48-6
(S)-2-((3aR)-4t-acetoxy-7a-methyl-(3ar,7at)-hexahydro-indan-1t-yl)-propan-1-ol

: 119569-20-9
(3aR)-1t-((S)-1,5-dimethyl-hexyl)-4t-(3,5-dinitro-benzoyloxy)-7a-methyl-(3ar,7at)-hexahydro-indan

Guidance literature:: Multi-step reaction with 5 steps

1: CrO₃; pyridine

2: aq.-ethanolic H₂SO₄

3: diethyl ether; butyl lithium / anschliessendes Erhitzen mit Dioxan und Erwaermen des Reaktionsprodukts mit Acetanhydrid und Kaliumacetat

4: platinum; acetic acid / Hydrogenation_.Erwaermen des Reaktionsprodukts mit methanol. Kalilauge

With pyridine; chromium(VI) oxide; n-butyllithium; diethyl ether; sulfuric acid; acetic acid; platinum;

Reference yield:

: 172227-33-7
<1R-(1α,3aβ,4α,7aα)>-4-acetoxyoctahydro-1-<(1R,2E,4R)-1,4,5-trimethyl-2-hexenyl>-7a-methyl-1H-indene

: 119569-20-9
(3aR)-1t-((S)-1,5-dimethyl-hexyl)-4t-(3,5-dinitro-benzoyloxy)-7a-methyl-(3ar,7at)-hexahydro-indan

Guidance literature:: Multi-step reaction with 6 steps

1: ozone; methanol / anschliessend Behandeln mit wss. NaBH₄

2: CrO₃; pyridine

3: aq.-ethanolic H₂SO₄

4: diethyl ether; butyl lithium / anschliessendes Erhitzen mit Dioxan und Erwaermen des Reaktionsprodukts mit Acetanhydrid und Kaliumacetat

5: platinum; acetic acid / Hydrogenation_.Erwaermen des Reaktionsprodukts mit methanol. Kalilauge

With pyridine; chromium(VI) oxide; methanol; n-butyllithium; diethyl ether; sulfuric acid; ozone; acetic acid; platinum;

Reference yield:

: 111411-27-9
2-((1E,3aR)-4t-acetoxy-7a-methyl-(3ar,7at)-hexahydro-indan-1-ylidene)-propionaldehyde

: 119569-20-9
(3aR)-1t-((S)-1,5-dimethyl-hexyl)-4t-(3,5-dinitro-benzoyloxy)-7a-methyl-(3ar,7at)-hexahydro-indan

Guidance literature:: Multi-step reaction with 5 steps

1: lithium; liquid NH₃

2: aq.-ethanolic H₂SO₄

3: diethyl ether; butyl lithium / anschliessendes Erhitzen mit Dioxan und Erwaermen des Reaktionsprodukts mit Acetanhydrid und Kaliumacetat

4: platinum; acetic acid / Hydrogenation_.Erwaermen des Reaktionsprodukts mit methanol. Kalilauge

With n-butyllithium; diethyl ether; sulfuric acid; ammonia; lithium; acetic acid; platinum;