Grundmann's alcohol

Base Information

Chemical Name:Grundmann's alcohol
CAS No.:33813-99-9
Molecular Formula:C₁₈H₃₄O
Molecular Weight:266.467
Hs Code.:

Synonyms:Grundmann's alcohol

Suppliers and Price of Grundmann's alcohol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of Grundmann's alcohol

Chemical Property:

Purity/Quality:: min 99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Grundmann's alcohol

There total 1 articles about Grundmann's alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 84927-67-3
3β-O-(tert-butyldimethylsilyl)-7,8-dihydroxy-7,8-dihydrovitamin D3

: 33813-99-9
Grundmann's alcohol

: 96685-53-9
(2Z)-2-<(5S)-5-(tert-butyldimethylsilyloxy)-2-methylene-cyclohexylidene>-ethanol

Guidance literature:: With lead(IV) acetate; sodium bis(2-methoxyethoxy)aluminium dihydride; Yield given. Multistep reaction. Yields of byproduct given; 1.) benzene, pyridine, 25 deg C, 10 min, 2.) water, 1,5h;
DOI:10.1021/jo00157a004

Reference yield: 91.0%

: 33813-99-9
Grundmann's alcohol

: 2746-25-0
p-Methoxybenzyl bromide

: (1R,3aR,4S,7aR)-1-[(R)-1,5-dimethylhexyl]-4-(4-methoxybenzyloxy)-7a-methyloctahydro-1H-indene

Guidance literature:: Grundmann's alcohol; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; for 1h; Cooling;

p-Methoxybenzyl bromide; In N,N-dimethyl-formamide; mineral oil; at 120 ℃; for 12h; Cooling;
DOI:10.1002/cmdc.201700792

Reference yield: 88.0%

: 32078-38-9
4-allyloxybenzyl chloride

: 33813-99-9
Grundmann's alcohol

: (1R,3aR,4S,7aR)-1-[(R)-1,5-dimethylhexyl]-4-(4-allocbenzyloxy)-7a-methyloctahydro-1H-indene

Guidance literature:: Grundmann's alcohol; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; for 1h; Cooling;

4-allyloxybenzyl chloride; In N,N-dimethyl-formamide; mineral oil; at 120 ℃; for 12h; Cooling;
DOI:10.1002/cmdc.201700792