C₄₂H₅₆B₁₂ClNP₂Ru

Base Information

• Chemical Name: C₄₂H₅₆B₁₂ClNP₂Ru
• CAS No.: 107282-80-4
• Molecular Formula: C₄₂H₅₆B₁₂ClNP₂Ru
• Molecular Weight: 903.116

Synonyms:

Chemical Property of C₄₂H₅₆B₁₂ClNP₂Ru

Chemical Property:

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Technology Process of C₄₂H₅₆B₁₂ClNP₂Ru

There total 1 articles about C₄₂H₅₆B₁₂ClNP₂Ru which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

tris(triphenylphosphine)ruthenium(II) chloride (15529-49-4,41756-81-4) + bis(triethylammonium) closo-dodecahydroborate → C42H56B12ClNP2Ru (107282-80-4)

Guidance literature:

In ethanol; (NHEt3)2(B12H12) was dissolved in refluxing EtOH and Ru-complex was added, the mixt. was heated under reflux for 3 h, then the EtOH was removed under reduced pressure (50-60°C, rotary evaporator, H2O pump); the residue was purified by preparative thin layer chromy. using CH2Cl2-n-C5H12 as eluting medium;

DOI:10.1039/DT9870000451

upstream raw materials:

tris(triphenylphosphine)ruthenium(II) chloride

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