1,2,3,3a-tetrahydro-6,8-dimethyl-10-(3,5-dimethylphenyl)benzocyclopenta<8><1,2>diazepine

Base Information

Chemical Name:1,2,3,3a-tetrahydro-6,8-dimethyl-10-(3,5-dimethylphenyl)benzocyclopenta<8><1,2>diazepine
CAS No.:90862-87-6
Molecular Formula:C₂₂H₂₄N₂
Molecular Weight:316.446
Hs Code.:

1,2,3,3a-tetrahydro-6,8-dimethyl-10-(3,5-dimethylphenyl)benzo<c>cyclopenta<8><1,2>diazepine

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2,3,3a-tetrahydro-6,8-dimethyl-10-(3,5-dimethylphenyl)benzocyclopenta<8><1,2>diazepine

Chemical Property:

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Technology Process of 1,2,3,3a-tetrahydro-6,8-dimethyl-10-(3,5-dimethylphenyl)benzocyclopenta<8><1,2>diazepine

There total 4 articles about 1,2,3,3a-tetrahydro-6,8-dimethyl-10-(3,5-dimethylphenyl)benzocyclopenta<8><1,2>diazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 90862-77-4
2-cyclopentanone tosylhydrazone

: 90862-87-6
1,2,3,3a-tetrahydro-6,8-dimethyl-10-(3,5-dimethylphenyl)benzocyclopenta<8><1,2>diazepine

Guidance literature:: With sodium ethanolate; Yield given. Multistep reaction; 1.) ethanol, 1 h, in the dark, 2.) reflux;

Reference yield:

: 23153-73-3
ethyl 1,4-dioxaspiro[4,4]nonane-6-carboxylate

: 90862-87-6
1,2,3,3a-tetrahydro-6,8-dimethyl-10-(3,5-dimethylphenyl)benzocyclopenta<8><1,2>diazepine

Guidance literature:: Multi-step reaction with 3 steps

3: 1.) sodium ethoxide / 1.) ethanol, 1 h, in the dark, 2.) reflux

With sodium ethanolate;

Reference yield:

: 34696-73-6
3,5-dimethyphenylmagnesium bromide

: 90862-87-6
1,2,3,3a-tetrahydro-6,8-dimethyl-10-(3,5-dimethylphenyl)benzocyclopenta<8><1,2>diazepine

Guidance literature:: Multi-step reaction with 3 steps

3: 1.) sodium ethoxide / 1.) ethanol, 1 h, in the dark, 2.) reflux

With sodium ethanolate;