[Li(THF)4][((Me3Si)2N)4Sm4(μ4SEt)(μ-SEt)8]*C6H6

Base Information

Chemical Name:[Li(THF)4][((Me3Si)2N)4Sm4(μ4SEt)(μ-SEt)8]*C6H6
CAS No.:1020090-68-9
Molecular Formula:C₆H₆*C₁₆H₃₂LiO₄*C₄₂H₁₁₇N₄S₉Si₈Sm₄
Molecular Weight:2166.62
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Li(THF)4][((Me3Si)2N)4Sm4(μ4SEt)(μ-SEt)8]*C6H6

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Technology Process of [Li(THF)4][((Me3Si)2N)4Sm4(μ4SEt)(μ-SEt)8]*C6H6

There total 1 articles about [Li(THF)4][((Me3Si)2N)4Sm4(μ4SEt)(μ-SEt)8]*C6H6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: 548443-16-9
[Sm(bis(trimethylsilyl)amido)3(μ-Cl)Li(tetrahydrofuran)3]

: 75-08-1
ethanethiol

: 71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1
benzene

: 1020090-68-9
[Li(THF)4][((Me3Si)2N)4Sm4(μ4SEt)(μ-SEt)8]*C6H6

Guidance literature:: In tetrahydrofuran; benzene; soln. of EtSH added dropwise to soln. of Sm compd. (1:1), stirred at room temp. for 3 h; concd. (vac.), extd. (benzene), filtered, crystd. on cooling to 2°C for 1 wk, elem. anal.;
DOI:10.1002/ejic.200601132