4-Methyl-N-(2-methylbut-3-yn-2-yl)aniline

Base Information

Chemical Name:4-Methyl-N-(2-methylbut-3-yn-2-yl)aniline
CAS No.:14465-52-2
Molecular Formula:C₁₂H₁₅N
Molecular Weight:173.258
Hs Code.:2921430090
DSSTox Substance ID:DTXSID50542208
Nikkaji Number:J131.584F
Wikidata:Q82418795
Mol file:14465-52-2.mol

Synonyms:4-Methyl-N-(2-methylbut-3-yn-2-yl)aniline;14465-52-2;N-(1,1-Dimethyl-2-propynyl)-p-toluidine;DTXSID50542208

Suppliers and Price of 4-Methyl-N-(2-methylbut-3-yn-2-yl)aniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 4-Methyl-N-(2-methylbut-3-yn-2-yl)aniline

Chemical Property:

PSA：12.03000
LogP:2.89170
XLogP3:3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:173.120449483
Heavy Atom Count:13
Complexity:200

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)NC(C)(C)C#C

Technology Process of 4-Methyl-N-(2-methylbut-3-yn-2-yl)aniline

There total 2 articles about 4-Methyl-N-(2-methylbut-3-yn-2-yl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1111-97-3
3-chloro-3-methylbut-1-yne

: 106-49-0,12221-03-3
p-toluidine

: 14465-52-2
N-(1',1'-dimethyl-2'-propynyl)-4-methylaniline

Guidance literature:: DOI:10.1021/jo01037a042

Reference yield:

: 14465-52-2
N-(1',1'-dimethyl-2'-propynyl)-4-methylaniline

Guidance literature:: p-Toluidin, 3-Chlor-3-methyl-but-1-in / Cu, neben 2,2,6-Trimethyl-dihydrochinolin (II);

Reference yield:

: 14465-52-2
N-(1',1'-dimethyl-2'-propynyl)-4-methylaniline

: 2,N,N-trimethyl-4-(3'-tolyl)-2-butanamine

Guidance literature:: Multi-step reaction with 4 steps

1: 24 percent / decane / 216 h / 205 °C

2: 88 percent / H₂ / Raney-Ni / ethanol; hexane

3: 53 percent / Na₂CO₃ / H₂O / Ambient temperature

4: 62 percent / methanol / 3 h / Ambient temperature; Irradiation

With hydrogen; sodium carbonate; nickel; In methanol; decane; ethanol; hexane; water;
DOI:10.1002/hlca.19850680721