AZOBENZENE-3-CARBOXYLICACID

Base Information

Chemical Name:AZOBENZENE-3-CARBOXYLICACID
CAS No.:14474-22-7
Molecular Formula:C13H10N2O2
Molecular Weight:226.235
Hs Code.:2927000090
Mol file:14474-22-7.mol

Synonyms:Benzoic acid, 3-(phenylazo)-;3-phenylazo-benzoic acid;3-Benzolazo-benzoesaeure;3-Phenylazo-benzoesaeure;3-phenyldiazobenzoic acid;

Suppliers and Price of AZOBENZENE-3-CARBOXYLICACID

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of AZOBENZENE-3-CARBOXYLICACID

Chemical Property:

Melting Point:170-171 °C
Boiling Point:427.5±28.0 °C(Predicted)
PKA:3.88±0.10(Predicted)
PSA：62.02000
Density:1.19±0.1 g/cm3(Predicted)
LogP:3.80020

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of AZOBENZENE-3-CARBOXYLICACID

There total 7 articles about AZOBENZENE-3-CARBOXYLICACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 99-05-8,159139-79-4
meta-aminobenzoic acid

: 586-96-9
Nitrosobenzene

: 14474-22-7
3-phenylazobenzoic acid

Guidance literature:: With acetic acid; at 20 ℃; for 48h;
DOI:10.1002/chem.201102609

Reference yield:

: 99-05-8,159139-79-4
meta-aminobenzoic acid

: 14474-22-7
3-phenylazobenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: Oxone / dichloromethane; water

2: acetic acid

With Oxone; acetic acid; In dichloromethane; water;
DOI:10.1016/j.bmcl.2012.10.014