Diazene, (4-nitrophenyl)[4-(oxiranylmethoxy)phenyl]-

Base Information

Chemical Name:Diazene, (4-nitrophenyl)[4-(oxiranylmethoxy)phenyl]-
CAS No.:145191-01-1
Molecular Formula:C15H13N3O4
Molecular Weight:299.286
Hs Code.:
DSSTox Substance ID:DTXSID40389260
Mol file:145191-01-1.mol

Synonyms:Diazene, (4-nitrophenyl)[4-(oxiranylmethoxy)phenyl]-;145191-01-1;DTXSID40389260;AKOS000666632;AKOS024304155;4-(4-nitrophenylazo)phenyl glycidyl ether;SR-01000324020;SR-01000324020-1

Suppliers and Price of Diazene, (4-nitrophenyl)[4-(oxiranylmethoxy)phenyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Diazene, (4-nitrophenyl)[4-(oxiranylmethoxy)phenyl]-

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:5
Exact Mass:299.09060590
Heavy Atom Count:22
Complexity:396

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C(O1)COC2=CC=C(C=C2)N=NC3=CC=C(C=C3)[N+](=O)[O-]

Technology Process of Diazene, (4-nitrophenyl)[4-(oxiranylmethoxy)phenyl]-

There total 3 articles about Diazene, (4-nitrophenyl)[4-(oxiranylmethoxy)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1435-60-5,81944-71-0
4-(4'-hydroxyphenylazo)nitrobenzene

: 106-89-8,24969-06-0,13403-37-7
epichlorohydrin

: 145191-01-1
4-(4-nitrophenylazo)phenyl glycidyl ether

Guidance literature:: With sodium hydroxide; sodium carbonate; benzalkonium chloride; In water; at 55 - 60 ℃; for 3h;
DOI:10.1007/s11172-005-0431-0

Reference yield:

: 100-01-6,104810-17-5
4-nitro-aniline

: 145191-01-1
4-(4-nitrophenylazo)phenyl glycidyl ether

Guidance literature:: Multi-step reaction with 2 steps

1.1: HCl; NaNO₂ / H₂O / 0.5 h / 5 °C

1.2: 84 percent / sodium carbonate / H₂O / 0 - 60 °C

2.1: 73 percent / sodium carbonate; NaOH / katamine AB / H₂O / 3 h / 55 - 60 °C

With hydrogenchloride; sodium hydroxide; sodium carbonate; sodium nitrite; benzalkonium chloride; In water;
DOI:10.1007/s11172-005-0431-0

Reference yield:

: 108-95-2,27073-41-2
phenol

: 145191-01-1
4-(4-nitrophenylazo)phenyl glycidyl ether

Guidance literature:: Multi-step reaction with 2 steps

1.1: HCl; NaNO₂ / H₂O / 0.5 h / 5 °C

1.2: 84 percent / sodium carbonate / H₂O / 0 - 60 °C

2.1: 73 percent / sodium carbonate; NaOH / katamine AB / H₂O / 3 h / 55 - 60 °C

With hydrogenchloride; sodium hydroxide; sodium carbonate; sodium nitrite; benzalkonium chloride; In water;
DOI:10.1007/s11172-005-0431-0