(6R)-3-(1-methyl-1H-tetrazol-5-ylsulfanylmethyl)-7t-((Ξ)-2-nitro-benzenesulfinylamino)-8-oxo-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid

Base Information

• Chemical Name: (6R)-3-(1-methyl-1H-tetrazol-5-ylsulfanylmethyl)-7t-((Ξ)-2-nitro-benzenesulfinylamino)-8-oxo-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid
• CAS No.: 65269-28-5
• Molecular Formula: C₁₆H₁₅N₇O₆S₃
• Molecular Weight: 497.536

Synonyms:

Chemical Property of (6R)-3-(1-methyl-1H-tetrazol-5-ylsulfanylmethyl)-7t-((Ξ)-2-nitro-benzenesulfinylamino)-8-oxo-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid

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Technology Process of (6R)-3-(1-methyl-1H-tetrazol-5-ylsulfanylmethyl)-7t-((Ξ)-2-nitro-benzenesulfinylamino)-8-oxo-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid

There total 1 articles about (6R)-3-(1-methyl-1H-tetrazol-5-ylsulfanylmethyl)-7t-((Ξ)-2-nitro-benzenesulfinylamino)-8-oxo-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ (6R)-3-(1-methyl-1H-tetrazol-5-ylsulfanylmethyl)-7t-((Ξ)-2-nitro-benzenesulfinylamino)-8-oxo-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid (65269-28-5)

Guidance literature:

aus 7ss-Amino-3-(1-methyl-1H-tetrazol-5-yl)thiomethyl-4-carbonsaeure, o-Nitrobenzolsulfinylchlorid/Et3N;

Reference yield:

lithium methanolate (865-34-9) + (6R)-3-(1-methyl-1H-tetrazol-5-ylsulfanylmethyl)-7t-(2-nitro-benzene(Ξ)sulfinylamino)-8-oxo-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid (65269-28-5) → (6R)-7c-methoxy-3-(1-methyl-1H-tetrazol-5-ylsulfanylmethyl)-7t-(2-nitro-phenylsulfanylamino)-8-oxo-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid (65269-29-6)

Guidance literature:

Multistep reaction; (i) Me₃SiCl, Et₃N, CHCl₃, (ii) quinoline, SOCl₂, (iii) /BRN= 3552389/;

DOI:10.1248/cpb.27.2727

Downstream raw materials:

(6R)-7c-methoxy-3-(1-methyl-1H-tetrazol-5-ylsulfanylmethyl)-7t-(2-nitro-phenylsulfanylamino)-8-oxo-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid

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