2,2,6,6-Tetramethyl-4-(2-propynyloxy)piperidine 1-Oxyl Free Radical

Base Information

Chemical Name:2,2,6,6-Tetramethyl-4-(2-propynyloxy)piperidine 1-Oxyl Free Radical
CAS No.:147045-24-7
Molecular Formula:C12H20NO2
Molecular Weight:210.296
Hs Code.:
Mol file:147045-24-7.mol

Synonyms:4-(prop-2-ynyloxy)-2,2,6,6-tetramethylpiperidine-1-oxyl;4-(propargyloxy)-2,2,6,6-tetramethylpiperidin-1-oxyl;O-propargyl-TEMPO;4-(propargyloxy)-TEMPO;2,2,6,6-tetramethyl-4-(prop-2-ynyloxy)piperidin-1-oxyl;4-(propargyloxy)-2,2,6,6-tetramethylpiperidine N-oxide;4-propargyloxy-TEMPO;

Suppliers and Price of 2,2,6,6-Tetramethyl-4-(2-propynyloxy)piperidine 1-Oxyl Free Radical

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2,2,6,6-Tetramethyl-4-(2-propynyloxy)piperidine 1-Oxyl Free Radical
100mg
$ 75.00

TCI Chemical
2,2,6,6-Tetramethyl-4-(2-propynyloxy)piperidine 1-Oxyl Free Radical >98.0%(GC)(T)
1g
$ 105.00

TCI Chemical
2,2,6,6-Tetramethyl-4-(2-propynyloxy)piperidine 1-Oxyl Free Radical >98.0%(GC)(T)
5g
$ 367.00

AK Scientific
2,2,6,6-Tetramethyl-4-(2-propynyloxy)piperidine 1-Oxyl Free Radical
1g
$ 198.00

Total 7 raw suppliers

Chemical Property of 2,2,6,6-Tetramethyl-4-(2-propynyloxy)piperidine 1-Oxyl Free Radical

Chemical Property:

Melting Point:65.0 to 69.0 °C
PSA：12.47000
LogP:1.94120
Solubility.:soluble in Methanol

Purity/Quality:

97% ^*data from raw suppliers

2,2,6,6-Tetramethyl-4-(2-propynyloxy)piperidine 1-Oxyl Free Radical ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,2,6,6-Tetramethyl-4-(2-propynyloxy)piperidine 1-Oxyl Free Radical

There total 2 articles about 2,2,6,6-Tetramethyl-4-(2-propynyloxy)piperidine 1-Oxyl Free Radical which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.3%

: 45985-24-8,2226-96-2
TEMPOL

: 106-96-7
propargyl bromide

: 147045-24-7
4-(prop-2-ynyloxy)-2,2,6,6-tetramethylpiperidine-1-oxyl

Guidance literature:: TEMPOL; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 - 20 ℃; for 1h;

propargyl bromide; In tetrahydrofuran; mineral oil; at 0 - 20 ℃; for 24.75h;
DOI:10.1021/ma501613x

Reference yield: 64.0%

: 2226-96-2
tempol

: 106-96-7
propargyl bromide

: 147045-24-7
4-propargyloxy-TEMPO

Guidance literature:: tempol; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 1h;

propargyl bromide; In N,N-dimethyl-formamide; at 20 ℃; for 20h;
DOI:10.3987/COM-10-12027

Reference yield: 86.0%

: 147045-24-7
4-(prop-2-ynyloxy)-2,2,6,6-tetramethylpiperidine-1-oxyl

: C₄₆H₂₅F₅₁N₁₂O₃

: C₅₈H₄₅F₅₁N₁₃O₅

Guidance literature:: With copper(l) iodide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 26 - 27 ℃; for 72h; Inert atmosphere;
DOI:10.1021/ol801555f