Technology Process of Carbamic acid, [6-(3-chlorophenyl)-1,2-dihydro-2-oxo-3-pyridinyl]-,
phenylmethyl ester
There total 3 articles about Carbamic acid, [6-(3-chlorophenyl)-1,2-dihydro-2-oxo-3-pyridinyl]-,
phenylmethyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium methylate / 1.) acetonitrile, reflux, 2.) DMF, 100 deg C
2: hydrogen bromide / acetic acid / Heating
3: diphenyl-phosphinic acid; triethylamine / 1,4-dioxane / Heating
4: 1,4-dioxane / Heating
With
diphenyl-phosphinic acid; hydrogen bromide; sodium methylate; triethylamine;
In
1,4-dioxane; acetic acid;
DOI:10.1021/jm00046a015
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrogen bromide / acetic acid / Heating
2: diphenyl-phosphinic acid; triethylamine / 1,4-dioxane / Heating
3: 1,4-dioxane / Heating
With
diphenyl-phosphinic acid; hydrogen bromide; triethylamine;
In
1,4-dioxane; acetic acid;
DOI:10.1021/jm00046a015
- Guidance literature:
-
Multi-step reaction with 2 steps
1: diphenyl-phosphinic acid; triethylamine / 1,4-dioxane / Heating
2: 1,4-dioxane / Heating
With
diphenyl-phosphinic acid; triethylamine;
In
1,4-dioxane;
DOI:10.1021/jm00046a015
