Benzoic acid, 4-(octadecyloxy)-, 4-aminophenyl ester

Base Information

• Chemical Name: Benzoic acid, 4-(octadecyloxy)-, 4-aminophenyl ester
• CAS No.: 147622-40-0
• Molecular Formula: C31H47NO3
• Molecular Weight: 481.719
• Mol file: 147622-40-0.mol

Synonyms:

Chemical Property of Benzoic acid, 4-(octadecyloxy)-, 4-aminophenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzoic acid, 4-(octadecyloxy)-, 4-aminophenyl ester

There total 5 articles about Benzoic acid, 4-(octadecyloxy)-, 4-aminophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

4-nitrophenyl-4'-octadecyloxybenzoate (157836-35-6) → 4-<(4'-octadecyloxyphenyl)benzoate>aminophenyl (147622-40-0)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; dichloromethane; under 3420 Torr;

DOI:10.1016/S0040-4039(00)77514-9

Reference yield:

4-(octadecyloxy)benzoic acid (15872-50-1) → 4-<(4'-octadecyloxyphenyl)benzoate>aminophenyl (147622-40-0)

Guidance literature:

Multi-step reaction with 2 steps

1: DCC; DMAP / CH₂Cl₂

2: H₂ / Pd/C / benzene / atmospheric pressure

With dmap; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In dichloromethane; benzene;

DOI:10.1039/b316731c

Reference yield:

methyl 4-(octadecyloxy)benzoate (40654-37-3) → 4-<(4'-octadecyloxyphenyl)benzoate>aminophenyl (147622-40-0)

Guidance literature:

Multi-step reaction with 3 steps

1: KOH / ethanol / Heating

2: DCC; DMAP / CH₂Cl₂

3: H₂ / Pd/C / benzene / atmospheric pressure

With dmap; potassium hydroxide; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In ethanol; dichloromethane; benzene;

DOI:10.1039/b316731c

upstream raw materials:

4-nitrophenyl-4'-octadecyloxybenzoate

4-(octadecyloxy)benzoic acid

methyl 4-(octadecyloxy)benzoate

methyl 4-hydroxylbenzoate

Downstream raw materials:

C₇₇H₁₀₃N₃O₆