Technology Process of Oxirane, 3-(bromomethyl)-2-methyl-2-phenyl-
There total 5 articles about Oxirane, 3-(bromomethyl)-2-methyl-2-phenyl- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
for 3h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 89.5 percent / diisopropylaluminium hydride / diethyl ether; hexane / 12 h / Ambient temperature
2: 78.1 percent / N-bromosuccinimide, Me2S / CH2Cl2 / 1) -10 deg C, 2 h, 2) room temperature, 1 h
3: 93 percent / m-chloroperbenzoic acid / CH2Cl2 / 3 h
With
N-Bromosuccinimide; diisopropyl aluminum hydride; dimethylsulfide; 3-chloro-benzenecarboperoxoic acid;
In
diethyl ether; hexane; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: toluene-p-sulfonic acid / toluene / Heating
2: 89.5 percent / diisopropylaluminium hydride / diethyl ether; hexane / 12 h / Ambient temperature
3: 78.1 percent / N-bromosuccinimide, Me2S / CH2Cl2 / 1) -10 deg C, 2 h, 2) room temperature, 1 h
4: 93 percent / m-chloroperbenzoic acid / CH2Cl2 / 3 h
With
N-Bromosuccinimide; diisopropyl aluminum hydride; dimethylsulfide; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid;
In
diethyl ether; hexane; dichloromethane; toluene;
