Cu(OCC(C(CH₃)3)CHC(C(CH₃)3)CHCNNCCNO₂(CH)4)2

Base Information

• Chemical Name: Cu(OCC(C(CH₃)3)CHC(C(CH₃)3)CHCNNCCNO₂(CH)4)2
• CAS No.: 132012-57-8
• Molecular Formula: C₄₀H₄₈CuN₆O₆
• Molecular Weight: 772.404

Synonyms:

Chemical Property of Cu(OCC(C(CH₃)3)CHC(C(CH₃)3)CHCNNCCNO₂(CH)4)2

Chemical Property:

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Technology Process of Cu(OCC(C(CH₃)3)CHC(C(CH₃)3)CHCNNCCNO₂(CH)4)2

There total 1 articles about Cu(OCC(C(CH₃)3)CHC(C(CH₃)3)CHCNNCCNO₂(CH)4)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

copper(II) acetate tetrahydrate + 2,4-bis(1,1-dimethylethyl)-6-[(2-nitrophenyl)diazenyl]phenol (52184-14-2) → Cu(OCC(C(CH3)3)CHC(C(CH3)3)CHCNNCCNO2(CH)4)2 (132012-57-8)

Guidance literature:

In ethanol; water; mixing equivalent amts. of aq. soln. of Cu(Acet)2*4H2O and ethanolic soln. of the azo ligand at 50-60°C;

Reference yield:

Cu(OCC(C(CH3)3)CHC(C(CH3)3)CHCNNCCNO2(CH)4)2 (132012-57-8) + Tri(p-tolyl)phosphine (1038-95-5,218281-19-7) → Cu(OCC(C(CH3)3)CHC(C(CH3)3)CHCNNCCNO2(CH)4)(P(C(CH)2CCH3(CH)2)3)2

Guidance literature:

In toluene; react. of Cu-complex with an excess of PPh3-derivative in toluene at room temp., absence of O2;

Reference yield:

Cu(OCC(C(CH3)3)CHC(C(CH3)3)CHCNNCCNO2(CH)4)2 (132012-57-8) + tri(m-chlorophenyl)-phosphine (29949-85-7) → Cu(OCC(C(CH3)3)CHC(C(CH3)3)CHCNNCCNO2(CH)4)(P(CCHCCl(CH)3)3)2

Guidance literature:

In toluene; react. of Cu-complex with an excess of PPh3-derivative in toluene at room temp., absence of O2;

upstream raw materials:

2,4-bis(1,1-dimethylethyl)-6-[(2-nitrophenyl)diazenyl]phenol

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