3-(propan-2-yl)naphthalen-2-yl acetate

Base Information

• Chemical Name: 3-(propan-2-yl)naphthalen-2-yl acetate
• CAS No.: 60683-45-6
• Molecular Formula: C₁₅H₁₆O₂
• Molecular Weight: 228.291
• Mol file: 60683-45-6.mol

Synonyms:2-Naphthalenol,3-(1-methylethyl)-, acetate (9CI); 2-Acetoxy-3-isopropylnaphthalene; NSC 168011

Chemical Property of 3-(propan-2-yl)naphthalen-2-yl acetate

Chemical Property:

• Vapor Pressure: 0.000183mmHg at 25°C
• Boiling Point: 328.9°C at 760 mmHg
• Flash Point: 115°C
• Density: 1.08g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-(propan-2-yl)naphthalen-2-yl acetate

There total 4 articles about 3-(propan-2-yl)naphthalen-2-yl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-acetoxy-3-isopropenylnaphthalene (60683-44-5) → 2-acetoxy-3-isopropylnaphthalene (60683-45-6)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; for 17h; Ambient temperature;

DOI:10.1246/bcsj.61.911

Reference yield:

3-hydroxy-2-naphthoic acid methyl ester (883-99-8) → 2-acetoxy-3-isopropylnaphthalene (60683-45-6)

Guidance literature:

Multi-step reaction with 3 steps

1: diethyl ether / 1.5 h / Heating

2: 96 percent / sodium acetate / 7 h / Heating

3: 10.366 g / H₂ / Pd/C / methanol / 17 h / Ambient temperature

With hydrogen; sodium acetate; palladium on activated charcoal; In methanol; diethyl ether;

DOI:10.1246/bcsj.61.911

Reference yield:

3-(1'-hydroxy-1'-methylethyl)-2-naphthol (859947-04-9) → 2-acetoxy-3-isopropylnaphthalene (60683-45-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 96 percent / sodium acetate / 7 h / Heating

2: 10.366 g / H₂ / Pd/C / methanol / 17 h / Ambient temperature

With hydrogen; sodium acetate; palladium on activated charcoal; In methanol;

DOI:10.1246/bcsj.61.911

upstream raw materials:

2-acetoxy-3-isopropenylnaphthalene

3-hydroxy-2-naphthoic acid methyl ester

3-(1'-hydroxy-1'-methylethyl)-2-naphthol

Downstream raw materials:

1,1-bis(benzoyloxy)-3-isopropyl-2(1H)-naphthalenone

2,2-bis(benzoyloxy)-3-isopropyl-1(2H)-naphthalenone

1-benzoyloxy-3-isopropyl-2-naphthol

2-benzoyloxy-3-isopropyl-1-naphthol