5,8-Tridecadiyn-7-one

Base Information

Chemical Name:5,8-Tridecadiyn-7-one
CAS No.:18621-56-2
Molecular Formula:C₁₃H₁₈O
Molecular Weight:190.285
Hs Code.:2914190090
NSC Number:94549
DSSTox Substance ID:DTXSID50171870
Nikkaji Number:J2.734.609J
Wikidata:Q83042020
Mol file:18621-56-2.mol

Synonyms:5,8-Tridecadiyn-7-one;trideca-5,8-diyn-7-one;18621-56-2;BRN 1857058;NSC94549;NCIOpen2_001312;SCHEMBL16594184;DTXSID50171870;NSC 94549;NSC-94549

Suppliers and Price of 5,8-Tridecadiyn-7-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 5,8-Tridecadiyn-7-one

Chemical Property:

Vapor Pressure:0.00397mmHg at 25°C
Boiling Point:279.6°Cat760mmHg
Flash Point:111.5°C
PSA：17.07000
Density:0.919g/cm³
LogP:2.94270
XLogP3:5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:190.135765193
Heavy Atom Count:14
Complexity:256

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCC#CC(=O)C#CCCCC

Technology Process of 5,8-Tridecadiyn-7-one

There total 6 articles about 5,8-Tridecadiyn-7-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1401246-05-6
(S)-3-(hex-1-yn-1-yl)non-4-yne-2,3-diol

: 18621-56-2
trideca-5,8-diyn-7-one

Guidance literature:: With SiO₂-supported NaIO₄; In Isopropyl acetate; at 20 ℃; Green chemistry;
DOI:10.1039/c8gc03275k

Reference yield: 73.0%

: 18621-55-1
trideca-5,8-diyn-7-ol

: 18621-56-2
trideca-5,8-diyn-7-one

Guidance literature:: With 4 A molecular sieve; pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1002/chem.200204584

Reference yield: 73.0%

: 693-02-7
hex-1-yne

: 109-94-4
formic acid ethyl ester

: 18621-56-2
trideca-5,8-diyn-7-one

Guidance literature:: hex-1-yne; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere; Schlenk technique; Glovebox;

formic acid ethyl ester; In tetrahydrofuran; at -78 - 20 ℃; for 1h; Inert atmosphere; Schlenk technique; Glovebox;

With dipyridinium dichromate; In dichloromethane; at 20 ℃; Inert atmosphere; Schlenk technique; Glovebox;
DOI:10.1021/ja504892c