Cyclohexyldichlorophosphine sulfide

Base Information

• Chemical Name: Cyclohexyldichlorophosphine sulfide
• CAS No.: 1498-63-1
• Molecular Formula: C6H11Cl2PS
• Molecular Weight: 217.099
• Hs Code.: 2930909090
• DSSTox Substance ID: DTXSID30400478
• Nikkaji Number: J1.197.665D
• Wikidata: Q82203480
• Mol file: 1498-63-1.mol

Synonyms:1498-63-1;Cyclohexyldichlorophosphine sulfide;CYCLOHEXYLPHOSPHONOTHIOIC DICHLORIDE;dichloro-cyclohexyl-sulfanylidene-lambda5-phosphane;Phosphonothioic dichloride, cyclohexyl-;SCHEMBL8139368;DTXSID30400478

Chemical Property of Cyclohexyldichlorophosphine sulfide

Chemical Property:

• PSA: 41.90000
• LogP: 4.75680
• XLogP3: 4.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 215.9696139
• Heavy Atom Count: 10
• Complexity: 148

Purity/Quality:

99% ^*data from raw suppliers

CYCLOHEXYLPHOSPHONOTHIOIC DICHLORIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CCC(CC1)P(=S)(Cl)Cl

Technology Process of Cyclohexyldichlorophosphine sulfide

There total 3 articles about Cyclohexyldichlorophosphine sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclohexylphosphonic dichloride (1005-22-7) → cyclohexylthiophosphonic acid dichloride (1498-63-1)

Guidance literature:

With tetraphosphorus decasulfide;

DOI:10.1007/BF01083802 DOI:10.1097/01.LAB.0000017165.26718.60

Reference yield:

cyclohexyl chloride (542-18-7) → cyclohexylthiophosphonic acid dichloride (1498-63-1)

Guidance literature:

With aluminium chloride dimer; water; thiourea; phosphorus trichloride; Yield given. Multistep reaction; CH₂Cl₂;

DOI:10.1021/jo01299a053

Reference yield:

→ cyclohexylthiophosphonic acid dichloride (1498-63-1)

Guidance literature:

Phosphonousdichlorid I, Schwefel, SnCl4;

upstream raw materials:

cyclohexylphosphonic dichloride

cyclohexyl chloride

Downstream raw materials:

bis(cyclohexylphosphonotrithioic) bisthioanhydride

Cyclohexyl-phosphonothioic acid S-propyl ester O-(2,4,6-tribromo-phenyl) ester

Cyclohexyl-phosphonothioic acid O-(4-nitro-phenyl) ester S-propyl ester

Cyclohexyl-phosphonothioic acid O-(2,4-dichloro-phenyl) ester S-propyl ester