1H-Inden-1-one

Base Information

• Chemical Name: 1H-Inden-1-one
• CAS No.: 480-90-0
• Molecular Formula: C9H6O
• Molecular Weight: 130.146
• Hs Code.: 2914700090
• Mol file: 480-90-0.mol

Synonyms:Indone (6CI,8CI);Inden-1-one;

Chemical Property of 1H-Inden-1-one

Chemical Property:

• Vapor Pressure: 0.0176mmHg at 25°C
• Melting Point: 0 °C
• Refractive Index: 1.622
• Boiling Point: 254.1 °C at 760 mmHg
• Flash Point: 105.3 °C
• PSA: 17.07000
• Density: 1.201 g/cm³
• LogP: 1.89610

Purity/Quality:

99%, ^*data from raw suppliers

1H-Inden-1-one ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1H-Inden-1-one

There total 51 articles about 1H-Inden-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.6%

2-indenone ethylene ketal (6710-43-6) → 1H-inden-1-one (480-90-0)

Guidance literature:

With toluene-4-sulfonic acid; In tetrahydrofuran; water; for 6h; Ambient temperature;

DOI:10.1021/ja00530a039

Reference yield: 94.0%

inden-1-one (83-33-0) → 1H-inden-1-one (480-90-0) + 3-Bromoindan-1-one (40774-41-2)

Guidance literature:

With N-Bromosuccinimide; In acetonitrile; at 20 ℃; for 0.216667h; Flow reactor; Irradiation; Large scale;

DOI:10.1021/jo402409k

Reference yield: 93.0%

3-Hydroxyindene (61463-21-6,109380-06-5,109431-69-8,112836-60-9,56631-57-3) → 1H-inden-1-one (480-90-0)

Guidance literature:

With chloro{bis-N,N'-(salicylaldehyde)ethylenediiminato}chromium(III); [bis(acetoxy)iodo]benzene; In dichloromethane; at 20 ℃; for 5h;

DOI:10.1021/ol000142y

upstream raw materials:

3-Hydroxyindene

3-Bromoindan-1-one

inden-1-yl hydroperoxide

1-indene

Downstream raw materials:

2,3-dibromo-indan-1-one

9H-indeno<2,1-c>phenanthren-9-one

13H-indeno<1,2-c>phenanthren-13-one

1a,6a-dihydro-1-oxacyclopropa[a]inden-6-one

Refernces

• 1、 Stultz, Laura K.,Huynh, My Hang V.,Binstead, Robert A.,Curry, Maria,Meyer, Thomas J.. "Allylic oxidation of cyclohexene and indene by cis-[Ru(IV)(bpy)2 (py)(O)]2+". . p. 5984 - 5996. Retrieved 2000.
• 2、 Erden, Ihsan,G?rtner, Christian,Ma, Jingxiang,Cabrera, Gabriel,Markham, Kate,Azimi, Saeed,Gronert, Scott. "Cyclopentadienones via a Tandem C-Cyclopropylnitrone Cyclization-Cycloreversion Sequence". . p. 5147 - 5153. Retrieved 2017.
• 3、 Deutscher, Jennifer,Gerschel, Philipp,Warm, Katrin,Kuhlmann, Uwe,Mebs, Stefan,Haumann, Michael,Dau, Holger,Hildebrandt, Peter,Apfel, Ulf-Peter,Ray, Kallol. "A bioinspired oxoiron(iv) motif supported on a N2S2macrocyclic ligand". supporting information. p. 2947 - 2950. Retrieved 2021/03/24.
• 4、 Fadaei Sarabi, Mahsa,Bezaatpour, Abolfazl,Mahmoudi, Ali. "Anchoring of a terpyridine-based Mo(VI) complex on manganese ferrite as a recoverable catalyst for epoxidation of olefins under solvent-free conditions". . p. 1597 - 1612. Retrieved 2021/03/29.