bis(trimethylsilyl)-α-benzyl phosphonate

Base Information

• Chemical Name: bis(trimethylsilyl)-α-benzyl phosphonate
• CAS No.: 125889-03-4
• Molecular Formula: C₁₈H₃₄NO₃PSi₂
• Molecular Weight: 399.618

Synonyms:

Chemical Property of bis(trimethylsilyl)-α-benzyl phosphonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of bis(trimethylsilyl)-α-benzyl phosphonate

There total 4 articles about bis(trimethylsilyl)-α-benzyl phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(1-chloro-2,2-dimethylpropylidene)benzylamine (125889-00-1) → bis(trimethylsilyl)-α-benzyl phosphonate (125889-03-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 65 percent

2: 31 percent / 2 h / 160 °C

3: 2 h / 180 °C / isomerization

Reference yield:

tris(trimethylsilyl) phosphite (1795-31-9) → bis(trimethylsilyl)-α-benzyl phosphonate (125889-03-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 65 percent

2: 31 percent / 2 h / 160 °C

3: 2 h / 180 °C / isomerization

Reference yield:

bis(trimethylsilyl)-N-benzyl-2,2-dimethylpropanimidoyl phosphonate (125889-01-2) → bis(trimethylsilyl)-α-benzyl phosphonate (125889-03-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 31 percent / 2 h / 160 °C

2: 2 h / 180 °C / isomerization

upstream raw materials:

bis(trimethylsilyl)-N-benzylideneamino-2,2-dimethylpropyl phosphonate

tris(trimethylsilyl) phosphite

N-(1-chloro-2,2-dimethylpropylidene)benzylamine

bis(trimethylsilyl)-N-benzyl-2,2-dimethylpropanimidoyl phosphonate

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