3,6-dibromo-9-hexyl-9H-carbazole

Base Information

• Chemical Name: 3,6-dibromo-9-hexyl-9H-carbazole
• CAS No.: 150623-72-6
• Molecular Formula: C18H19Br2N
• Molecular Weight: 409.164
• European Community (EC) Number: 833-857-1
• DSSTox Substance ID: DTXSID10479187
• Nikkaji Number: J1.509.215G
• Wikidata: Q82313142
• Mol file: 150623-72-6.mol

Synonyms:3,6-dibromo-9-hexyl-9H-carbazole;150623-72-6;9H-Carbazole, 3,6-dibromo-9-hexyl-;3,6-DIBROMO-9-HEXYLCARBAZOLE;SCHEMBL3823482;DTXSID10479187;POMJRCRJZRALHK-UHFFFAOYSA-N;MFCD23099108;BS-43893;D5410;T70319

Chemical Property of 3,6-dibromo-9-hexyl-9H-carbazole

Chemical Property:

• Melting Point: 98.0 to 102.0 °C
• Boiling Point: 486.3±38.0 °C(Predicted)
• PSA: 4.93000
• Density: 1.50±0.1 g/cm3(Predicted)
• LogP: 6.89980
• XLogP3: 7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 5
• Exact Mass: 408.98638
• Heavy Atom Count: 21
• Complexity: 309

Purity/Quality:

97% ^*data from raw suppliers

3,6-Dibromo-9-hexyl-9H-carbazole ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCN1C2=C(C=C(C=C2)Br)C3=C1C=CC(=C3)Br

Technology Process of 3,6-dibromo-9-hexyl-9H-carbazole

There total 7 articles about 3,6-dibromo-9-hexyl-9H-carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

N-hexylcarbazole (4041-21-8) → 3,6-dibromo-9-hexyl-9H-carbazole (150623-72-6)

Guidance literature:

With N-Bromosuccinimide; In chloroform; at 40 ℃; for 12h;

Reference yield: 95.0%

3,6-dibromo-9H-carbazole (6825-20-3) + 1-bromo-hexane (111-25-1) → 3,6-dibromo-9-hexyl-9H-carbazole (150623-72-6)

Guidance literature:

With tetrabutylammomium bromide; potassium hydroxide; In water; at 20 ℃; for 0.5h;

DOI:10.1016/j.tetlet.2009.12.136

Reference yield:

9H-carbazole (86-74-8,105184-46-1,97960-57-1) → 3,6-dibromo-9-hexyl-9H-carbazole (150623-72-6)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydride / N,N-dimethyl-formamide / 6 h / 20 °C

2: bromine / dichloromethane / 12 h / 20 °C

With bromine; sodium hydride; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1080/15421406.2011.601189

upstream raw materials:

3,6-dibromo-9H-carbazole

1-bromo-hexane

N-hexylcarbazole

9H-carbazole

Downstream raw materials:

4,4'-(9-hexyl-9H-carbazole-3,6-diyl)dibenzaldehyde

3,6-di-(4-nitrophenyl)-9-hexyl-9H-carbazole

3,6-diphenyl-9-hexyl-9H-carbazole

9-hexyl-3,6-di(pyren-1-yl)carbazole

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