Ethanamine, 2-(diphenylarsino)-N,N-bis[2-(diphenylarsino)ethyl]-

Base Information

Chemical Name:Ethanamine, 2-(diphenylarsino)-N,N-bis[2-(diphenylarsino)ethyl]-
CAS No.:15114-56-4
Molecular Formula:C₄₂H₄₂As₃N
Molecular Weight:785.567
Hs Code.:
Mol file:15114-56-4.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethanamine, 2-(diphenylarsino)-N,N-bis[2-(diphenylarsino)ethyl]-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
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MSDS Files:: SDS file from LookChem

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Technology Process of Ethanamine, 2-(diphenylarsino)-N,N-bis[2-(diphenylarsino)ethyl]-

There total 2 articles about Ethanamine, 2-(diphenylarsino)-N,N-bis[2-(diphenylarsino)ethyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 817-09-4
tris-(2-chloroethyl)amine hydrochloride

: 41006-64-8
Natrium-diphenylarsenid

: 15114-56-4
tris(2-diphenylarsinoethyl)amin

Guidance literature:: With ammonia; Yield given. Multistep reaction; 1.) THF, 2.) ether, reflux, 3 h;
DOI:10.1016/0022-328X(83)80079-5

Reference yield:

: 15114-56-4
tris(2-diphenylarsinoethyl)amin

Guidance literature:: N(CH2-CH2Cl)3, Ph2AsK;
DOI:10.1002/9780470132470.ch47

Reference yield: 65.0%

: 23777-40-4
bis(triphenylphosphine)ethylenenickel⁽⁰⁾

: 15114-56-4
tris(2-diphenylarsinoethyl)amin

: 51778-20-2,58003-32-0
1,2,3-triphenylcyclopropenylium perchlorate

: triphenylphosphine[tris(2-diphenylarsinoethyl)amine]nickel(I) perchlorate

Guidance literature:: In tetrahydrofuran; methanol; under N2, soln. of (C3Ph3)ClO4 in boiling MeOH was added to soln. of Ni-complex (molar ratio 1:1) in THF, 1 equiv of solid ligand was added, heated at 50°C; filtered, washed with MeOH and light petroleum, dried under stream of N2; elem. anal.;
DOI:10.1039/DT9830002263