Benzoic acid, 2-hydroxy-5-[(E)-[(2-hydroxyphenyl)methylene]amino]-

Base Information

Chemical Name:Benzoic acid, 2-hydroxy-5-[(E)-[(2-hydroxyphenyl)methylene]amino]-
CAS No.:151391-75-2
Molecular Formula:C14H11NO4
Molecular Weight:257.24100
Hs Code.:
Mol file:151391-75-2.mol

Synonyms:2-Hydroxy-5-{[1-(2-hydroxy-phenyl)-meth-(E)-ylidene]-amino}-benzoic acid;5-{[(1E)-(2-hydroxyphenyl)methylene]amino}-2-hydroxybenzoic acid;

Suppliers and Price of Benzoic acid, 2-hydroxy-5-[(E)-[(2-hydroxyphenyl)methylene]amino]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzoic acid, 2-hydroxy-5-[(E)-[(2-hydroxyphenyl)methylene]amino]-

Chemical Property:

PSA：90.12000
LogP:2.54660

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzoic acid, 2-hydroxy-5-[(E)-[(2-hydroxyphenyl)methylene]amino]-

There total 2 articles about Benzoic acid, 2-hydroxy-5-[(E)-[(2-hydroxyphenyl)methylene]amino]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 89-95-2
2-methyl-benzyl alcohol

: 89-57-6
5-Aminosalicylic Acid

: 151391-75-2
5-{[(1E)-(2-hydroxyphenyl)methylene]amino}-2-hydroxybenzoic acid

Guidance literature:: In ethanol;

Reference yield:

: 89-57-6
5-Aminosalicylic Acid

: 90-02-8
salicylaldehyde

: 151391-75-2
5-{[(1E)-(2-hydroxyphenyl)methylene]amino}-2-hydroxybenzoic acid

Guidance literature:: With triethylamine; In methanol; at 60 ℃; for 8h;
DOI:10.1021/jm00077a014

Reference yield: 95.0%

: 557-34-6
zinc diacetate

: 151391-75-2
5-{[(1E)-(2-hydroxyphenyl)methylene]amino}-2-hydroxybenzoic acid

: 873784-80-6
(HOOCC₆H₃OHNCHC₆H₄O)2Zn

Guidance literature:: In ethanol; to an ethanol soln. of metal acetate was added an ethanol-soln. of salicyl-compound, the mixt. was heated at reflux for 3 h; ppt. was collected by suction filtration, washed with cold ethanol and diethyl ether, dried; elem. anal.;
DOI:10.1139/v05-091