1,3,5-Trichloro-2-ethynylbenzene

Base Information

Chemical Name:1,3,5-Trichloro-2-ethynylbenzene
CAS No.:152174-09-9
Molecular Formula:C8H3Cl3
Molecular Weight:205.471
Hs Code.:
DSSTox Substance ID:DTXSID90598527
Wikidata:Q82494294
Mol file:152174-09-9.mol

Synonyms:1,3,5-trichloro-2-ethynylbenzene;152174-09-9;2,4,6-Trichlorophenylacetylene;SCHEMBL3859125;DTXSID90598527;IAEFAPDXQDZALB-UHFFFAOYSA-N;2-Ethynyl-1,3,5-trichlorobenzene;MFCD11655770;AKOS012332562;CS-0266203;EN300-1254702

Suppliers and Price of 1,3,5-Trichloro-2-ethynylbenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 1,3,5-Trichloro-2-ethynylbenzene

Chemical Property:

XLogP3:4.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:1
Exact Mass:203.930033
Heavy Atom Count:11
Complexity:169

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C#CC1=C(C=C(C=C1Cl)Cl)Cl

Technology Process of 1,3,5-Trichloro-2-ethynylbenzene

There total 4 articles about 1,3,5-Trichloro-2-ethynylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 6324-50-1
1,3,5-trichloro-2-iodobenzene

: 1066-54-2
trimethylsilylacetylene

: 152174-09-9
1,3,5-trichloro-2-ethynylbenzene

Guidance literature:: 1,3,5-trichloro-2-iodobenzene; With bis-triphenylphosphine-palladium(II) chloride; triethylamine; for 0.166667h;

trimethylsilylacetylene; With copper(l) iodide; at 110 ℃; for 24h; Inert atmosphere; Sealed tube;

With potassium carbonate; In methanol; for 1h;
DOI:10.1055/s-0034-1378737

Reference yield: 20.7%

: triphenyl-(2,4,6-trichloro-phenylethynyl)-silane

: 152174-09-9
1,3,5-trichloro-2-ethynylbenzene

Guidance literature:: triphenyl-(2,4,6-trichloro-phenylethynyl)-silane; With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 0.5h;

With water; In diethyl ether;