Benzeneethaneselenothioic acid, S-butyl ester

Base Information

• Chemical Name: Benzeneethaneselenothioic acid, S-butyl ester
• CAS No.: 152554-82-0
• Molecular Formula: C12H16SSe
• Molecular Weight: 271.285
• Mol file: 152554-82-0.mol

Synonyms:

Chemical Property of Benzeneethaneselenothioic acid, S-butyl ester

Chemical Property:

Purity/Quality:

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Technology Process of Benzeneethaneselenothioic acid, S-butyl ester

There total 2 articles about Benzeneethaneselenothioic acid, S-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

n-butanethiol (109-79-5) + Se-Phenylethynyl selenoacetate (128010-20-8) → 1-Butylsulfanyl-2-phenyl-ethaneselone (152554-82-0)

Guidance literature:

With trifluoroacetic acid; In tetrahydrofuran; at 66 ℃; for 48h;

DOI:10.1021/ja970462l

Reference yield:

n-butanethiol (109-79-5) + phenylacetylene (536-74-3) → 1-Butylsulfanyl-2-phenyl-ethaneselone (152554-82-0)

Guidance literature:

With selenium; n-butyllithium; Yield given. Multistep reaction;

DOI:10.1246/cl.1993.1469

Reference yield: 85.0%

1-Butylsulfanyl-2-phenyl-ethaneselone (152554-82-0) + methyl iodide (74-88-4) → ((Z)-2-Butylsulfanyl-2-methylselanyl-vinyl)-benzene

Guidance literature:

With cadmium(II) acetate; triethylamine; In methanol; at 65 ℃; for 3h;

DOI:10.1246/cl.1996.877

upstream raw materials:

n-butanethiol

phenylacetylene

Se-Phenylethynyl selenoacetate

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