Disilane, 1,2-dichloro-1,1,2,2-tetraphenyl-

Base Information

• Chemical Name: Disilane, 1,2-dichloro-1,1,2,2-tetraphenyl-
• CAS No.: 15288-62-7
• Molecular Formula: C24H20Cl2Si2
• Molecular Weight: 435.5
• European Community (EC) Number: 888-090-5
• DSSTox Substance ID: DTXSID30464954
• Wikidata: Q82290538
• Mol file: 15288-62-7.mol

Synonyms:15288-62-7;Disilane, 1,2-dichloro-1,1,2,2-tetraphenyl-;1,2-Dichlortetraphenyldisilan;SCHEMBL9979264;DTXSID30464954;1,2-Dichloro-1,1,2,2-tetraphenyldisilane

Chemical Property of Disilane, 1,2-dichloro-1,1,2,2-tetraphenyl-

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 5
• Exact Mass: 434.0480591
• Heavy Atom Count: 28
• Complexity: 393

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)[Si](C2=CC=CC=C2)([Si](C3=CC=CC=C3)(C4=CC=CC=C4)Cl)Cl

Technology Process of Disilane, 1,2-dichloro-1,1,2,2-tetraphenyl-

There total 4 articles about Disilane, 1,2-dichloro-1,1,2,2-tetraphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

1,2-bis(diethylamino)-1,1,2,2-tetraphenyldisilane (157558-28-6) → 1,2-dichloro-1,1,2,2-tetraphenyldisilane (15288-62-7)

Guidance literature:

With acetyl chloride; In dichloromethane; at 20 ℃; for 24h;

DOI:10.1515/znb-2002-0703

Reference yield:

1,1,2,2-tetraphenyldisilane (16343-18-3) → 1,2-dichloro-1,1,2,2-tetraphenyldisilane (15288-62-7)

Guidance literature:

With phosphorus pentachloride; In tetrachloromethane;

DOI:10.1039/j19700001641

Reference yield:

2,3-dimethyl-buta-1,3-diene (513-81-5) + 1,3-dichloro-1,1-bis[2-(dimethylaminomethyl)phenyl]-2,2,3,3-tetraphenyltrisilane → 1,2-dichloro-1,1,2,2-tetraphenyldisilane (15288-62-7) + bis<<2-(N,N-dimethylamino)methyl>phenyl>3,4-dimethylsilacyclopent-3-ene

Guidance literature:

at 110 ℃; for 13h;

DOI:10.1016/S0022-328X(01)01451-6

upstream raw materials:

1,1,2,2-tetraphenyldisilane

2,3-dimethyl-buta-1,3-diene

1,2-bis(diethylamino)-1,1,2,2-tetraphenyldisilane

Downstream raw materials:

1,2-dimethyl-1,1,2,2-tetraphenyldisilane

1,1,2,2-tetraphenyldisilane-1,2-diol

1,1,2,2-tetraphenyl-1,2-disilacyclohexane

cis-1,6-diphenyl-1,6-disilabicyclo[4.4.0]decane