AKOS BBS-00008108

Base Information

• Chemical Name: AKOS BBS-00008108
• CAS No.: 15460-12-5
• Molecular Formula: C10H12Br2O
• Molecular Weight: 308.013
• Hs Code.: 2908199090
• Mol file: 15460-12-5.mol

Synonyms:2,4-dibromo-6-(tert-butyl)phenol;4,6-dibromo-2-t-butyl phenol;2,4-dibromo-6-t-butylphenol;

Chemical Property of AKOS BBS-00008108

Chemical Property:

• PSA: 20.23000
• LogP: 4.21470

Purity/Quality:

99% ^*data from raw suppliers

2,4-Dibromo-6-tert-butylphenol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of AKOS BBS-00008108

There total 9 articles about AKOS BBS-00008108 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

2-tert-Butylphenol (88-18-6) → 2,4-dibromo-6-tert-butylphenol (15460-12-5)

Guidance literature:

With N-Bromosuccinimide; triphenylphosphine sulfide; In dichloromethane; at 20 ℃; for 12h;

DOI:10.1055/s-0037-1609581

Reference yield: 2.0%

2-tert-Butylphenol (88-18-6) → 2-bromo-6-(tert-butyl)phenol (23159-87-7) + 2,4-dibromo-6-tert-butylphenol (15460-12-5) + 4-bromo-2-tert-butylphenol (10323-39-4)

Guidance literature:

With 4-morpholineethanesulfonic acid; V_BrPO(AnI) bromoperoxidase; dihydrogen peroxide; sodium bromide; In water; tert-butyl alcohol; at 23 ℃; pH=6.2; Overall yield = 44 %;

DOI:10.1039/c3dt51582f

Reference yield:

DBtBP + 2-tert-Butylphenol (88-18-6) → 2,4-dibromo-6-tert-butylphenol (15460-12-5)

Guidance literature:

With bromine; In water; ethyl acetate;

upstream raw materials:

2-tert-Butylphenol

2-bromo-6-(tert-butyl)phenol

2-(tert-butyl)-4-iodophenol

2-bromo-6-tert-butyl-4-iodophenol

Downstream raw materials:

2-Brom-6-tert.-butyl-1,4-benzochinon

1,5-Dibromo-3-tert-butyl-2-(3-methyl-but-2-enyloxy)-benzene

2,4-dibromo-6-tert-butylphenyl 1-cyclopent-1-enylmethyl ether

1,5-dibromo-(2-bromoethoxy)-3-tert-butylbenzene