Indolo[1,2-b]isoquinolin-6(11H)-one, 8,9,10-trimethoxy-12-(phenylthio)-

Base Information

Chemical Name:Indolo[1,2-b]isoquinolin-6(11H)-one, 8,9,10-trimethoxy-12-(phenylthio)-
CAS No.:154885-40-2
Molecular Formula:C25H21NO4S
Molecular Weight:431.512
Hs Code.:
Mol file:154885-40-2.mol

Synonyms:

Suppliers and Price of Indolo[1,2-b]isoquinolin-6(11H)-one, 8,9,10-trimethoxy-12-(phenylthio)-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Indolo[1,2-b]isoquinolin-6(11H)-one, 8,9,10-trimethoxy-12-(phenylthio)-

Chemical Property:

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Technology Process of Indolo[1,2-b]isoquinolin-6(11H)-one, 8,9,10-trimethoxy-12-(phenylthio)-

There total 7 articles about Indolo[1,2-b]isoquinolin-6(11H)-one, 8,9,10-trimethoxy-12-(phenylthio)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 154885-39-9
2-bromomethyl-3-phenylthio-1-(3,4,5-trimethoxybenzoyl)indole

: 154885-40-2
5-oxo-11-phenylthio-1,2,3-trimethoxyisoquinolono<2,3-a>indole

Guidance literature:: With copper dichloride; palladium dichloride; In acetonitrile; for 6h; Heating;
DOI:10.1055/s-1994-25456

Reference yield:

: 56366-45-1
2-methyl-3-phenylthioindole

: 154885-40-2
5-oxo-11-phenylthio-1,2,3-trimethoxyisoquinolono<2,3-a>indole

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / NaH / tetrahydrofuran / 4 h / Ambient temperature

2: 91 percent / NBS, dibenzoyl peroxide / CCl₄ / 2 h / Heating

3: 58 percent / PdCl₂, CuCl₂ / acetonitrile / 6 h / Heating

With N-Bromosuccinimide; sodium hydride; copper dichloride; palladium dichloride; dibenzoyl peroxide; In tetrahydrofuran; tetrachloromethane; acetonitrile;
DOI:10.1055/s-1994-25456

Reference yield:

: 5042-53-5
1-(phenylsulfanyl)acetone

: 154885-40-2
5-oxo-11-phenylthio-1,2,3-trimethoxyisoquinolono<2,3-a>indole

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / acetic acid / 3 h / Heating

2: 80 percent / NaH / tetrahydrofuran / 4 h / Ambient temperature

3: 91 percent / NBS, dibenzoyl peroxide / CCl₄ / 2 h / Heating

4: 58 percent / PdCl₂, CuCl₂ / acetonitrile / 6 h / Heating

With N-Bromosuccinimide; sodium hydride; copper dichloride; palladium dichloride; dibenzoyl peroxide; In tetrahydrofuran; tetrachloromethane; acetic acid; acetonitrile;
DOI:10.1055/s-1994-25456