Benzene, 1-[(1,1-dimethylethyl)sulfonyl]-2-[methoxy(3-methoxyphenyl)methyl]-

Base Information

Chemical Name:Benzene, 1-[(1,1-dimethylethyl)sulfonyl]-2-[methoxy(3-methoxyphenyl)methyl]-
CAS No.:155496-71-2
Molecular Formula:C₁₉H₂₄O₄S
Molecular Weight:348.463
Hs Code.:
Mol file:155496-71-2.mol

Synonyms:

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Chemical Property of Benzene, 1-[(1,1-dimethylethyl)sulfonyl]-2-[methoxy(3-methoxyphenyl)methyl]-

Chemical Property:

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Technology Process of Benzene, 1-[(1,1-dimethylethyl)sulfonyl]-2-[methoxy(3-methoxyphenyl)methyl]-

There total 6 articles about Benzene, 1-[(1,1-dimethylethyl)sulfonyl]-2-[methoxy(3-methoxyphenyl)methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3019-19-0
tert-butyl phenyl sulfide

: 155496-71-2
tert-butyl 2-phenyl sulfone

Guidance literature:: Multi-step reaction with 3 steps

1: sodium perborate tetrahydrate / acetic acid / 3 h / 50 °C

2: 1.) BuLi / 1) THF, hexane, -70 deg C, 30 min; 2) THF, hexane, -70 deg C --> room temperature, 2 h

3: 1.) NaH / 1) THF₀ deg C, 20 min; 2) THF, room temperature

With sodium perborate; n-butyllithium; sodium hydride; In acetic acid;

Reference yield:

: 108-98-5
thiophenol

: 155496-71-2
tert-butyl 2-phenyl sulfone

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / Amberlyst H-15 / diethyl ether / 72 h / -78 - 20 °C

2: sodium perborate tetrahydrate / acetic acid / 3 h / 50 °C

3: 1.) BuLi / 1) THF, hexane, -70 deg C, 30 min; 2) THF, hexane, -70 deg C --> room temperature, 2 h

4: 1.) NaH / 1) THF₀ deg C, 20 min; 2) THF, room temperature

With sodium perborate; n-butyllithium; Amberlyst H-15; sodium hydride; In diethyl ether; acetic acid;

Reference yield:

: 4170-72-3
tert-butyl-phenyl sulfone

: 155496-71-2
tert-butyl 2-phenyl sulfone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) BuLi / 1) THF, hexane, -70 deg C, 30 min; 2) THF, hexane, -70 deg C --> room temperature, 2 h

2: 1.) NaH / 1) THF₀ deg C, 20 min; 2) THF, room temperature

With n-butyllithium; sodium hydride;