p-fluorophenylxenon (m-fluorophenyl)2difluoroborate

Base Information

Chemical Name:p-fluorophenylxenon (m-fluorophenyl)2difluoroborate
CAS No.:144474-21-5
Molecular Formula:C₆H₄FXe*C₁₂H₈BF₄
Molecular Weight:465.386
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-fluorophenylxenon (m-fluorophenyl)2difluoroborate

Chemical Property:

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Technology Process of p-fluorophenylxenon (m-fluorophenyl)2difluoroborate

There total 3 articles about p-fluorophenylxenon (m-fluorophenyl)2difluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13709-36-9
xenon difluoride

: 47196-74-7
tris(4-fluorophenyl)borane

: 144474-21-5
p-fluorophenylxenon (m-fluorophenyl)2difluoroborate

Guidance literature:: In dichloromethane; (under dry Ar); FEP apparatus; addn. of solid XeF2 to a stirred soln. of the boron compd. in CH2Cl2 at -50°C, pptn. after several min; ppt. sepd., washed and dried in vac. at -50°C;

Reference yield:

: xenon fluoride

: 47196-74-7
tris(4-fluorophenyl)borane

: 144474-21-5
p-fluorophenylxenon (m-fluorophenyl)2difluoroborate

: 154069-44-0
p-fluorophenylxenon p-fluorophenyltrifluoroborate

Guidance literature:: In dichloromethane; addn. of solid XeF2 to soln. of B-compd. in CH2Cl2 at -60°C with stirring (under Ar), further addn. of solid XeF2 causes precipitation of product; washing with CH2Cl2 at -78°C, centrifugation, high vac. drying at -45°C;

Reference yield:

: xenon fluoride

: 47196-74-7
tris(4-fluorophenyl)borane

: 144474-21-5
p-fluorophenylxenon (m-fluorophenyl)2difluoroborate

: 147069-73-6
{Xe(4-FC₆H₄)}{BF₄}

: 154069-44-0
p-fluorophenylxenon p-fluorophenyltrifluoroborate

Guidance literature:: In dichloromethane; addn. of solid XeF2 to soln. of B-compd. in CH2Cl2 at -40°C with stirring (under Ar), further addn. of solid XeF2 causes precipitation of product; washing with CH2Cl2 at -78°C, centrifugation, high vac. drying at -45°C;