5-chloro-2-ethoxyaniline

Base Information

• Chemical Name: 5-chloro-2-ethoxyaniline
• CAS No.: 15793-48-3
• Molecular Formula: C8H10ClNO
• Molecular Weight: 171.626
• Hs Code.: 2922299090
• Mol file: 15793-48-3.mol

Synonyms:o-Phenethidine,5-chloro;5-chloro-2-ethoxyphenylamine;2-Aethoxy-5-chlor-anilin;HMS1703M01;Benzenamine, 5-chloro-2-ethoxy-;2-ethoxy-5-chloro-aniline;3-chloro-6-ethoxyaniline;5-chloro-2-ethoxy-benzenamine;5-Chlor-o-phenetidin;

Chemical Property of 5-chloro-2-ethoxyaniline

Chemical Property:

• Vapor Pressure: 0.00548mmHg at 25°C
• Melting Point: 21-22 °C
• Boiling Point: 274.2oC at 760 mmHg
• PKA: 3.42±0.10(Predicted)
• Flash Point: 119.6oC
• PSA: 35.25000
• Density: 1.19g/cm3
• LogP: 2.90210

Purity/Quality:

98%min ^*data from raw suppliers

5-Chloro-2-ethoxy-phenylamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-chloro-2-ethoxyaniline

There total 7 articles about 5-chloro-2-ethoxyaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-chloro-2-nitro-phenetole (102236-24-8) → 5-chloro-2-ethoxy aniline (15793-48-3)

Guidance literature:

With hydrogenchloride; iron;

Reference yield:

2-fluoro-5-chloronitrobenzene (345-18-6) → 5-chloro-2-ethoxy aniline (15793-48-3)

Guidance literature:

Multi-step reaction with 2 steps

1: KHMDS / tetrahydrofuran / 0 - 20 °C

2: aq. Na₂S₂O₄ / methanol / 0.17 h / 100 °C / microwave iradiation

With sodium dithionite; potassium hexamethylsilazane; In tetrahydrofuran; methanol;

DOI:10.1016/j.bmcl.2007.08.050

Reference yield:

4-chloro-2-nitro-phenetole (102236-24-8) → 5-chloro-2-ethoxy aniline (15793-48-3) + N,N'-bis-(2-ethoxy-5-chloro-phenyl)-hydrazine (855394-52-4)

Guidance literature:

With sodium hydroxide; lead(II) oxide; xylene; at 80 ℃; Reduktion an Eisen-Kathoden;

upstream raw materials:

2'-ethoxyacetanilide

N,N'-bis-(2-ethoxy-5-chloro-phenyl)-hydrazine

4-chloro-2-nitro-phenetole

ethyl bromide

Downstream raw materials:

N-(5-chloro-2-ethoxyphenyl)-1-benzofuran-2-sulfonamide

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