disalicylaldehyde phthaloyldihydrazone

Base Information

• Chemical Name: disalicylaldehyde phthaloyldihydrazone
• CAS No.: 112008-80-7
• Molecular Formula: C₂₂H₁₈N₄O₄
• Molecular Weight: 402.409
• Mol file: 112008-80-7.mol

Synonyms:

Chemical Property of disalicylaldehyde phthaloyldihydrazone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of disalicylaldehyde phthaloyldihydrazone

There total 1 articles about disalicylaldehyde phthaloyldihydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phthaloyldihydrazine (3645-45-2) + salicylaldehyde (90-02-8) → disalicylaldehyde phthaloyldihydrazone (112008-80-7)

Guidance literature:

Heating;

Reference yield:

uranyl(VI) acetate dihydrate + disalicylaldehyde phthaloyldihydrazone (112008-80-7) → {(UO2)2(OC6H4CHNNHC(O)C6H4C(O)NHNCHC6H4OH)2(CH3COO)2(CH3CH2OH)2}*CH3CH2OH

Guidance literature:

With ethanol; acetic acid; In ethanol; metal to ligand ratio 3:1, stirring, reflux (1 h); filtration, washing (1. ethanol/benzene, 2. benzene), drying over anhydrous CaCl2, elem. anal.;

Reference yield:

uranyl nirate hexahydrate + disalicylaldehyde phthaloyldihydrazone (112008-80-7) → {(UO2)2(OC6H4CHNNHC(O)C6H4C(O)NHNCHC6H4OH)2(NO3)2(H2O)4}*2H2O

Guidance literature:

In ethanol; metal to ligand ratio 3:1, stirring, reflux (2 h); filtration, washing (1. ethanol/benzene, 2. benzene), drying over anhydrous CaCl2, elem. anal.;

upstream raw materials:

phthaloyldihydrazine

salicylaldehyde