tetraphenylarsonium p-bromophenylthiochromate

Base Information

Chemical Name:tetraphenylarsonium p-bromophenylthiochromate
CAS No.:129554-57-0
Molecular Formula:C₆H₄BrCrO₃S*C₂₄H₂₀As
Molecular Weight:671.406
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tetraphenylarsonium p-bromophenylthiochromate

Chemical Property:

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Technology Process of tetraphenylarsonium p-bromophenylthiochromate

There total 2 articles about tetraphenylarsonium p-bromophenylthiochromate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: sodium dichromate dihydrate

: 507-27-7
tetraphenylarsonium bromide

: 106-53-6
para-bromobenzenethiol

: 129554-57-0
tetraphenylarsonium p-bromophenylthiochromate

Guidance literature:: In N,N-dimethyl-formamide; byproducts: H2O; at 0°C; isolated from DMF/ether, elem. anal.;
DOI:10.1016/S0277-5387(00)83765-1

Reference yield:

: 15912-80-8,763019-84-7
Tetraphenylarsonium

: 13907-47-6
dichromate anion

: 106-53-6
para-bromobenzenethiol

: 129554-57-0
tetraphenylarsonium p-bromophenylthiochromate

Guidance literature:: In N,N-dimethyl-formamide; pptn. by addn. of Et2O, recrystn. from DMF/Et2O; elem. anal.;
DOI:10.1016/S0277-5387(00)80290-9

Reference yield:

: 129554-57-0
tetraphenylarsonium p-bromophenylthiochromate

: 106-53-6
para-bromobenzenethiol

: 1233764-80-1
Cr(V)O₂(p-bromobenzenethiolate)2^(1-)

: 1233764-81-2
Cr(V)O(p-bromobenzenethiolate)4^(1-)

Guidance literature:: In dimethylsulfoxide-d6; byproducts: H2O; (dark); reaction chromium compd. and thiol deriv. in anhyd. DMSO-d6 at 295 K; UV and ESR monitoring; Kinetics;
DOI:10.1021/ja101675w