Phosphine, methyl[2,4,6-tris(1-methylethyl)phenyl]-

Base Information

Chemical Name:Phosphine, methyl[2,4,6-tris(1-methylethyl)phenyl]-
CAS No.:158748-69-7
Molecular Formula:C16H27P
Molecular Weight:250.364
Hs Code.:
DSSTox Substance ID:DTXSID70418799
Nikkaji Number:J1.823.579J
Wikidata:Q82229487
Mol file:158748-69-7.mol

Synonyms:158748-69-7;Phosphine, methyl[2,4,6-tris(1-methylethyl)phenyl]-;SCHEMBL6063611;DTXSID70418799;ZCHULNFSBXALBE-UHFFFAOYSA-N;methyl 2,4,6-triisopropylphenylphosphine;Methyl(2,4,6-triisopropylphenyl)phosphine #;Phosphine, methyl-(2,4,6-triisopropylphenyl)-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phosphine, methyl[2,4,6-tris(1-methylethyl)phenyl]-

Chemical Property:

XLogP3:4.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:4
Exact Mass:250.185037859
Heavy Atom Count:17
Complexity:202

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)C1=CC(=C(C(=C1)C(C)C)PC)C(C)C

Technology Process of Phosphine, methyl[2,4,6-tris(1-methylethyl)phenyl]-

There total 4 articles about Phosphine, methyl[2,4,6-tris(1-methylethyl)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 676-83-5
methyldichlorophosphane

: phenylmagnesium bromide

: 108894-99-1
(2,4,6-triisopropylphenyl)magnesium bromide

: 104108-09-0
Methyl-phenyl-(2,4,6-triisopropyl-phenyl)-phosphane

: 158748-69-7
PHMe(Is)

Guidance literature:: methyldichlorophosphane; (2,4,6-triisopropylphenyl)magnesium bromide; In diethyl ether; at -78 ℃;

phenylmagnesium bromide; In tetrahydrofuran; diethyl ether; at -78 - 20 ℃; Further stages.;
DOI:10.1021/ja0267324

Reference yield:

: [Cu((R,R)-Me-FerroLANE)(PHMe(Is))][PF₆]

: 1,1'-bis[(2R,5R)-2,5-dimethylphospholano]ferrocene

: Cu((R,R)-Me-FerroLANE)(PMeIs)

: 158748-69-7
PHMe(Is)

Guidance literature:: With sodium trimethylsilanolate; In tetrahydrofuran-d8; at -35 ℃; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/acs.inorgchem.9b01263

Reference yield:

: C₅₇H₉₃P₄Rh

: C₅₇H₉₃P₄Rh

: 158748-69-7
PHMe(Is)

Guidance literature:: In ⁽²⁾H₈-toluene; at 90 ℃; for 48h; Overall yield = 94 %; Overall yield = 94 mg; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.organomet.7b00515