[1,1'-Biphenyl]-2-sulfonamide, 4'-[[1-[5-amino-2-(trifluoromethyl)phenyl]-3-butyl-1,5-dihydro-5-oxo-4H-1 ,2,4-triazol-4-yl]methyl]-N-(1,1-dimethylethyl)-

Base Information

Chemical Name:[1,1'-Biphenyl]-2-sulfonamide, 4'-[[1-[5-amino-2-(trifluoromethyl)phenyl]-3-butyl-1,5-dihydro-5-oxo-4H-1 ,2,4-triazol-4-yl]methyl]-N-(1,1-dimethylethyl)-
CAS No.:159954-93-5
Molecular Formula:C30H34F3N5O3S
Molecular Weight:601.693
Hs Code.:
Mol file:159954-93-5.mol

[1,1'-Biphenyl]-2-sulfonamide,
4'-[[1-[5-amino-2-(trifluoromethyl)phenyl]-3-butyl-1,5-dihydro-5-oxo-4H-1
,2,4-triazol-4-yl]methyl]-N-(1,1-dimethylethyl)-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [1,1'-Biphenyl]-2-sulfonamide, 4'-[[1-[5-amino-2-(trifluoromethyl)phenyl]-3-butyl-1,5-dihydro-5-oxo-4H-1 ,2,4-triazol-4-yl]methyl]-N-(1,1-dimethylethyl)-

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Technology Process of [1,1'-Biphenyl]-2-sulfonamide, 4'-[[1-[5-amino-2-(trifluoromethyl)phenyl]-3-butyl-1,5-dihydro-5-oxo-4H-1 ,2,4-triazol-4-yl]methyl]-N-(1,1-dimethylethyl)-

There total 5 articles about [1,1'-Biphenyl]-2-sulfonamide, 4'-[[1-[5-amino-2-(trifluoromethyl)phenyl]-3-butyl-1,5-dihydro-5-oxo-4H-1 ,2,4-triazol-4-yl]methyl]-N-(1,1-dimethylethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 159547-16-7
5-n-Butyl-4-[[2'-(N-t-butylsulfamoyl)biphenyl-4-yl]methyl]-2,4-dihydro-2-[5-nitro-2-(trifluoromethyl)phenyl]-3H-1,2,4-triazol-3-one

: 159954-93-5
2-<5-amino-2-(trifluoromethyl)phenyl>-5-n-butyl-4-<<2'-(N-tert-butylsulfamoyl)biphenyl-4-yl>methyl>-2,4-dihydro-3H-1,2,4-triazol-3-one

Guidance literature:: With hydrogen; platinum(IV) oxide; In ethanol; ethyl acetate; under 3040 Torr;
DOI:10.1021/jm00052a006

Reference yield:

: 100367-78-0
(2-bromo-5-nitrophenyl)hydrazine

: 159954-93-5
2-<5-amino-2-(trifluoromethyl)phenyl>-5-n-butyl-4-<<2'-(N-tert-butylsulfamoyl)biphenyl-4-yl>methyl>-2,4-dihydro-3H-1,2,4-triazol-3-one

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N / toluene / 15 h / 90 °C

2: 1.) NaH / 1.) DMF, 50 deg C, 1 h, 2.) DMF, 50 deg C, 1.5 h

3: 37 percent / KF, CuI / dimethylformamide / 12 h / 120 °C

4: 100 percent / H₂ / PtO₂ / ethyl acetate; ethanol / 3040 Torr

With potassium fluoride; copper(l) iodide; hydrogen; sodium hydride; triethylamine; platinum(IV) oxide; In ethanol; ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm00052a006

Reference yield:

: 146949-06-6
ethyl N-carbethoxy-valerimidate

: 159954-93-5
2-<5-amino-2-(trifluoromethyl)phenyl>-5-n-butyl-4-<<2'-(N-tert-butylsulfamoyl)biphenyl-4-yl>methyl>-2,4-dihydro-3H-1,2,4-triazol-3-one

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N / toluene / 15 h / 90 °C

2: 1.) NaH / 1.) DMF, 50 deg C, 1 h, 2.) DMF, 50 deg C, 1.5 h

3: 37 percent / KF, CuI / dimethylformamide / 12 h / 120 °C

4: 100 percent / H₂ / PtO₂ / ethyl acetate; ethanol / 3040 Torr

With potassium fluoride; copper(l) iodide; hydrogen; sodium hydride; triethylamine; platinum(IV) oxide; In ethanol; ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm00052a006