Carbamic acid, N-(2-formylphenyl)-, methyl ester

Base Information

Chemical Name:Carbamic acid, N-(2-formylphenyl)-, methyl ester
CAS No.:160354-69-8
Molecular Formula:C9H9NO3
Molecular Weight:179.175
Hs Code.:
Mol file:160354-69-8.mol

Synonyms:(2-formyl-phenyl)-carbamic acid methyl ester;2-Carbomethoxyamino-benzaldehyd;methyl (2-formylphenyl)carbamate;2-(methyloxycarbonyl)aminobenzaldehyde;(2-Formyl-phenyl)-carbamidsaeure-methylester;Carbamic acid,(2-formylphenyl)-,methyl ester;

Suppliers and Price of Carbamic acid, N-(2-formylphenyl)-, methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Carbamic acid, N-(2-formylphenyl)-, methyl ester

Chemical Property:

PSA：58.89000
LogP:1.69100

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Carbamic acid, N-(2-formylphenyl)-, methyl ester

There total 4 articles about Carbamic acid, N-(2-formylphenyl)-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 117550-36-4
methyl ortho-(hydroxymethyl)phenyl carbamate

: 160354-69-8
2-(methyloxycarbonyl)aminobenzaldehyde

Guidance literature:: With aluminum oxide; pyridinium chlorochromate; In chloroform; for 0.5h; Ambient temperature;
DOI:10.1021/jo981816+

Reference yield:

: 5344-90-1
2-Aminobenzyl alcohol

: 160354-69-8
2-(methyloxycarbonyl)aminobenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / tetrahydrofuran; H₂O / 1 h / 20 °C

2: 6.9 g / MnO₂ / CH₂Cl₂ / 2 h

With manganese(IV) oxide; potassium carbonate; In tetrahydrofuran; dichloromethane; water;
DOI:10.1039/b611121a

Reference yield:

: 118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4
anthranilic acid

: 160354-69-8
2-(methyloxycarbonyl)aminobenzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere

2: sodium hydrogencarbonate / 1,4-dioxane; water / 2 h / 0 - 20 °C / Inert atmosphere

3: manganese(IV) oxide / dichloromethane / 4 h / 20 °C / Inert atmosphere

With manganese(IV) oxide; lithium aluminium tetrahydride; sodium hydrogencarbonate; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water;
DOI:10.1021/acs.orglett.8b00905