Benzonitrile, 4-[[tris(1-methylethyl)silyl]oxy]-

Base Information Edit

Chemical Name:Benzonitrile, 4-[[tris(1-methylethyl)silyl]oxy]-
CAS No.:160725-46-2
Molecular Formula:C16H25NOSi
Molecular Weight:275.466
Hs Code.:
Mol file:160725-46-2.mol

Synonyms:

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Chemical Property of Benzonitrile, 4-[[tris(1-methylethyl)silyl]oxy]- Edit

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MSDS Files:: SDS file from LookChem

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Technology Process of Benzonitrile, 4-[[tris(1-methylethyl)silyl]oxy]-

There total 1 articles about Benzonitrile, 4-[[tris(1-methylethyl)silyl]oxy]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 13154-24-0
triisopropylsilyl chloride

: 767-00-0
4-cyanophenol

: 160725-46-2
4-((triisopropylsilyl)oxy)benzonitrile

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 25 ℃; for 24h;
DOI:10.1016/0223-5234(94)90027-2

Reference yield: 63.0%

: 148259-35-2
tert-butyldimethyl(dibromomethyl)silane

: 160725-46-2
4-((triisopropylsilyl)oxy)benzonitrile

: 1-(t-butyldimethylsilyl)-2-(4-triisopropylsiloxyphenyl)ethane-1,2-dione

Guidance literature:: tert-butyldimethyl(dibromomethyl)silane; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 1h;

4-((triisopropylsilyl)oxy)benzonitrile; In tetrahydrofuran; at -78 ℃; for 1h;

With hydrogenchloride; In tetrahydrofuran;
DOI:10.1021/ja047708o