1-(5,6-Dimethyl-1h-benzotriazol-1-yl)ethanone

Base Information

Chemical Name:1-(5,6-Dimethyl-1h-benzotriazol-1-yl)ethanone
CAS No.:70740-21-5
Molecular Formula:C₁₀H₁₁N₃O
Molecular Weight:189.217
Hs Code.:
NSC Number:82628
DSSTox Substance ID:DTXSID20292440
Nikkaji Number:J1.495.066D
Wikidata:Q82030743

Synonyms:70740-21-5;1-(5,6-dimethyl-1h-benzotriazol-1-yl)ethanone;NSC82628;SCHEMBL19911450;DTXSID20292440;NSC-82628;1-(5,6-Dimethyl-1H-benzo[d][1,2,3]triazol-1-yl)ethanone

Suppliers and Price of 1-(5,6-Dimethyl-1h-benzotriazol-1-yl)ethanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 1-(5,6-Dimethyl-1h-benzotriazol-1-yl)ethanone

Chemical Property:

Vapor Pressure:7.31E-05mmHg at 25°C
Boiling Point:342.9°C at 760 mmHg
Flash Point:161.2°C
Density:1.24g/cm³
XLogP3:1.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:0
Exact Mass:189.090211983
Heavy Atom Count:14
Complexity:244

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC2=C(C=C1C)N(N=N2)C(=O)C

Technology Process of 1-(5,6-Dimethyl-1h-benzotriazol-1-yl)ethanone

There total 7 articles about 1-(5,6-Dimethyl-1h-benzotriazol-1-yl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 4184-79-6
5,6-dimethylbenzotriazole

: 75-36-5
acetyl chloride

: 70740-21-5
1-acetyl-5,6-dimethylbenzotriazole

Guidance literature:: With triethylamine; In dichloromethane;
DOI:10.1021/jo0009604

Reference yield:

: 117044-02-7
acetic acid-(2-amino-4,5-dimethyl-anilide)

: 70740-21-5
1-acetyl-5,6-dimethylbenzotriazole

Guidance literature:: With acetic acid; sodium nitrite;
DOI:10.1021/ja01139a053

Reference yield:

: 6970-77-0
N-(4,5-dimethyl-2-nitrophenyl)acetamide

: 70740-21-5
1-acetyl-5,6-dimethylbenzotriazole

Guidance literature:: Multi-step reaction with 2 steps

1: iron; acetic acid

2: aqueous acetic acid; NaNO₂

With iron; acetic acid; sodium nitrite;
DOI:10.1021/ja01139a053