4-[(Benzenesulfonyl)methyl]pyridine

Base Information

Chemical Name:4-[(Benzenesulfonyl)methyl]pyridine
CAS No.:1620-52-6
Molecular Formula:C12H11NO2S
Molecular Weight:233.28600
Hs Code.:
European Community (EC) Number:664-938-8
Nikkaji Number:J515.686F
Mol file:1620-52-6.mol

Synonyms:4-[(benzenesulfonyl)methyl]pyridine;4-(Phenylsulfonylmethyl)pyridine;PHENYL 4-PYRIDYLMETHYL SULFONE;AKOS024324026

Suppliers and Price of 4-[(Benzenesulfonyl)methyl]pyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
PHENYL 4-PYRIDYLMETHYL SULFONE Aldrich
250mg
$ 144.00

Total 1 raw suppliers

Chemical Property of 4-[(Benzenesulfonyl)methyl]pyridine

Chemical Property:

Melting Point:205 - 207 °C (CH2Cl2)
PSA：55.41000
LogP:3.13630
XLogP3:1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:233.05104977
Heavy Atom Count:16
Complexity:296

Purity/Quality:

95% ^*data from raw suppliers

PHENYL 4-PYRIDYLMETHYL SULFONE Aldrich ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)S(=O)(=O)CC2=CC=NC=C2

Technology Process of 4-[(Benzenesulfonyl)methyl]pyridine

There total 13 articles about 4-[(Benzenesulfonyl)methyl]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 147645-84-9
4-phenylsulfonylmethylpyridinium 1-dicyanomethylide

: 1620-52-6
4-((benzenesulfonyl)methyl)pyridine

Guidance literature:: With ammonium persulfate; In methanol; for 1h; Heating;
DOI:10.1248/cpb.41.220

Reference yield: 98.0%

: 873-55-2
sodium benzenesulfonate

: 1620-52-6
4-((benzenesulfonyl)methyl)pyridine

Guidance literature:: With tetra-n-propylammonium bromide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 80 ℃; for 24h;
DOI:10.1055/s-2004-822311

Reference yield: 62.0%

: 1120-87-2
4-bromopyridin

: 3112-85-4
methylphenylsulfonate

: 1620-52-6
4-((benzenesulfonyl)methyl)pyridine

Guidance literature:: methylphenylsulfonate; With lithium hexamethyldisilazane; In tetrahydrofuran; at -20 - 20 ℃; Inert atmosphere;

With zinc(II) chloride; In tetrahydrofuran; at -20 - 20 ℃; for 1h; Inert atmosphere;

4-bromopyridin; With palladium diacetate; XPhos; In tetrahydrofuran; at 65 ℃; Degassed under vacuum; Inert atmosphere;
DOI:10.1016/j.tetlet.2009.12.035