Rhenium, methyldioxoperoxy-

Base Information

• Chemical Name: Rhenium, methyldioxoperoxy-
• CAS No.: 162331-68-2
• Molecular Formula: CH3O4Re
• Molecular Weight: 265.239
• Mol file: 162331-68-2.mol

Synonyms:

Chemical Property of Rhenium, methyldioxoperoxy-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Rhenium, methyldioxoperoxy-

There total 6 articles about Rhenium, methyldioxoperoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dihydrogen peroxide (7722-84-1) + methyltrioxorhenium(VII) (70197-13-6) → methyldioxoperoxorhenium(VII) (162331-68-2) + water (7732-18-5)

Guidance literature:

In tetrahydrofuran-d8; 25°C;

DOI:10.1021/ja952305x

Reference yield:

water (7732-18-5) + dihydrogen peroxide (7722-84-1) + methyltrioxorhenium(VII) (70197-13-6) → methy(oxo)bis(η(2)-peroxo)rhenium(VII) (152385-10-9) + methyldioxoperoxorhenium(VII) (162331-68-2)

Guidance literature:

In [D₃]acetonitrile; water; varying concn. of water; not isolated, reaction followed by NMR spectroscopy; product ratio depending on water concn.;

DOI:10.1021/ic970650c

Reference yield:

dihydrogen peroxide (7722-84-1) + methyltrioxorhenium(VII) (70197-13-6) → methyl(oxo)diperoxorhenium(VII) (1144513-40-5,171078-32-3) + methyldioxoperoxorhenium(VII) (162331-68-2)

Guidance literature:

In tetrahydrofuran-d8; under Ar, Schlenk techniques; detected by NMR spectroscopy;

DOI:10.1039/b608219j

upstream raw materials:

dihydrogen peroxide

methyltrioxorhenium(VII)

water

methyl(oxo)diperoxorhenium(VII)

Downstream raw materials:

dihydrogen peroxide

methyltrioxorhenium(VII)

perrhenate