Magnesium,2-Phenyl-1,3-Dioxolane,Bromide

Base Information

Chemical Name:Magnesium,2-Phenyl-1,3-Dioxolane,Bromide
CAS No.:164718-49-4
Molecular Formula:C9H9BrMgO2
Molecular Weight:253.378
Hs Code.:
Mol file:164718-49-4.mol

Synonyms:bromo[2-(1,3-dioxolan-2-yl)phenyl]magnesium;BrMg(C6H4-2-CHO2C2H4);Magnesium,bromo[2-(1,3-dioxolan-2-yl)phenyl];(2-(1,3-dioxolan-2-yl)phenyl)-magnesium bromide;2-(1,3-dioxolanyl)phenylmagnesium bromide;

Suppliers and Price of Magnesium,2-Phenyl-1,3-Dioxolane,Bromide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Rieke Metals
2-(1,3-Dioxolan-2-yl)phenylmagnesiumbromide
100mL
$ 396.00

Rieke Metals
2-(1,3-Dioxolan-2-yl)phenylmagnesiumbromide
50mL
$ 226.00

Total 8 raw suppliers

Chemical Property of Magnesium,2-Phenyl-1,3-Dioxolane,Bromide

Chemical Property:

PSA：18.46000
LogP:-1.78110

Purity/Quality:

98% ^*data from raw suppliers

2-(1,3-Dioxolan-2-yl)phenylmagnesiumbromide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Magnesium,2-Phenyl-1,3-Dioxolane,Bromide

There total 2 articles about Magnesium,2-Phenyl-1,3-Dioxolane,Bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 34824-58-3
2-(2-bromophenyl)-1,3-dioxolan

: 164718-49-4
(2-(1,3-dioxolan-2-yl)phenyl)-magnesium bromide

Guidance literature:: With magnesium; In tetrahydrofuran;

Reference yield:

: 6630-33-7
ortho-bromobenzaldehyde

: 164718-49-4
(2-(1,3-dioxolan-2-yl)phenyl)-magnesium bromide

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / p-toluenesulfonic acid monohydrate / toluene / Heating

2: Mg / tetrahydrofuran

With toluene-4-sulfonic acid; magnesium; In tetrahydrofuran; toluene;

Reference yield: 75.0%

: 1421840-45-0
C₂₁H₁₉ClNO₄PS

: 164718-49-4
(2-(1,3-dioxolan-2-yl)phenyl)-magnesium bromide

: 1421840-47-2
(S)-4-chloro-2-[(1R)-1-{[(4-methylphenyl)sulfonyl]amino}ethyl]phenyl-2-(1,3-dioxolan-2-yl)phenyl(phenyl)phosphinate

Guidance literature:: C₂₁H₁₉ClNO₄PS; (2-(1,3-dioxolan-2-yl)phenyl)-magnesium bromide; In tetrahydrofuran; at -20 ℃; Inert atmosphere;

With ammonium chloride; In tetrahydrofuran; Inert atmosphere;
DOI:10.1021/ja312352p