Benzene, 1-(butylthio)-4-fluoro-

Base Information

Chemical Name:Benzene, 1-(butylthio)-4-fluoro-
CAS No.:1649-99-6
Molecular Formula:C10H13FS
Molecular Weight:184.278
Hs Code.:
DSSTox Substance ID:DTXSID20435254
Nikkaji Number:J427.635C
Wikidata:Q82250058
Mol file:1649-99-6.mol

Synonyms:Benzene, 1-(butylthio)-4-fluoro-;1649-99-6;(4-Fluorophenyl)butyl sulfide;SCHEMBL424976;DTXSID20435254;1-(BUTYLSULFANYL)-4-FLUOROBENZENE

Suppliers and Price of Benzene, 1-(butylthio)-4-fluoro-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Benzene, 1-(butylthio)-4-fluoro-

Chemical Property:

XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:184.07219975
Heavy Atom Count:12
Complexity:108

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCSC1=CC=C(C=C1)F

Technology Process of Benzene, 1-(butylthio)-4-fluoro-

There total 5 articles about Benzene, 1-(butylthio)-4-fluoro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 109-79-5
n-butanethiol

: 460-00-4
1-Bromo-4-fluorobenzene

: 1649-99-6
1-(butylsulfanyl)-4-fluorobenzene

Guidance literature:: n-butanethiol; With sodium t-butanolate; In xylene; at 0 - 20 ℃;

1-Bromo-4-fluorobenzene; With tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In xylene; at 140 ℃; for 0.4h;
DOI:10.1016/j.tet.2005.03.078

Reference yield: 91.0%

: 109-65-9
1-bromo-butane

: S-(4-fluorophenyl)isothiouronium 3,5-dinitrobenzoate

: 1649-99-6
1-(butylsulfanyl)-4-fluorobenzene

Guidance literature:: With potassium carbonate; In methanol; at 60 ℃; for 15h; Sealed tube; Inert atmosphere;
DOI:10.1002/chem.201901874

Reference yield:

: 542-69-8
1-iodo-butane

: 371-42-6
4-Fluorothiophenol

: 1649-99-6
1-(butylsulfanyl)-4-fluorobenzene

Guidance literature:: 4-Fluorothiophenol; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.166667h; Inert atmosphere;

1-iodo-butane; In N,N-dimethyl-formamide; Inert atmosphere; Reflux;
DOI:10.1039/c9cc06535k