(1Z)-1-Iodo-1-hexene

Base Information

• Chemical Name: (1Z)-1-Iodo-1-hexene
• CAS No.: 16538-47-9
• Molecular Formula: C6H11I
• Molecular Weight: 210.058
• Hs Code.: 2903399090
• Mol file: 16538-47-9.mol

Synonyms:1-iodohex-1-ene;(Z)-1-iodohexene;(Z)-1-iodohex-1-ene;(1Z)-1-iodo-hex-1-ene;cis-1-iodo-1-hexene;(Z)-1-iodo-1-hexene;

Chemical Property of (1Z)-1-Iodo-1-hexene

Chemical Property:

• Refractive Index: 1.4970 (estimate)
• Boiling Point: 151.64°C (estimate)
• PSA: 0.00000
• Density: 1.4517 (rough estimate)
• LogP: 3.12530

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (1Z)-1-Iodo-1-hexene

There total 29 articles about (1Z)-1-Iodo-1-hexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

(Z)-1-<(1',1'-dimethylethyl)diphenylsilyl>hex-1-ene (123628-87-5) → (Z)-1-iodohex-1-ene (16538-47-9)

Guidance literature:

With N-iodo-succinimide; In 1,1,1,3',3',3'-hexafluoro-propanol; at 0 ℃; Inert atmosphere; Darkness;

DOI:10.1021/ol2020187

Reference yield: 69.0%

(Z)-(1-iodo-1-hexenyl)trimethylsilane (76346-98-0) → (Z)-1-iodohex-1-ene (16538-47-9)

Guidance literature:

With sodium methylate; In tetrahydrofuran; methanol; at 25 ℃; for 4h;

DOI:10.1055/s-1981-29679

Reference yield: 60.0%

1-iodo-1-hexyne (1119-67-1) → (Z)-1-iodohex-1-ene (16538-47-9)

Guidance literature:

With bis(cyclohexanyl)borane; In tetrahydrofuran; at 0 ℃;

DOI:10.1021/ja00330a041

upstream raw materials:

(Z)-hex-1-enyl(trimethyl)silane

(E)-1-trimethylsilyl-1-hexene

1-iodo-1-hexyne

n-butyl magnesium bromide

Downstream raw materials:

(Z)-9-tetradecen-1-yl acetate

(Z)-oct-3-en-1-yne

(Z)-hex-1-en-1-ylbenzene

(E)-1-phenyl-1-hexene