1-p-tolylhexan-1-one

Base Information

• Chemical Name: 1-p-tolylhexan-1-one
• CAS No.: 1669-33-6
• Molecular Formula: C13H18O
• Molecular Weight: 190.285
• Mol file: 1669-33-6.mol

Synonyms:p-Methyl-caprophenon;1-(p-tolyl)hexan-1-one;4-Methylcaprophenon;1-(4-tolyl)-1-hexanone;1-p-tolyl-hexan-1-one;p-tolyl pentyl ketone;

Chemical Property of 1-p-tolylhexan-1-one

Chemical Property:

• Melting Point: 39.5-40.5 °C(Solv: methanol (67-56-1))
• Boiling Point: 130-135 °C(Press: 4 Torr)
• PSA: 17.07000
• Density: 0.936±0.06 g/cm3(Predicted)
• LogP: 3.75800
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

96% ^*data from raw suppliers

1-p-Tolyl-hexan-1-one ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-p-tolylhexan-1-one

There total 17 articles about 1-p-tolylhexan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

1-(4-methylphenyl)-1-hexanol (71434-61-2) → pentyl 4-methylphenyl ketone (1669-33-6)

Guidance literature:

With acrylic acid methyl ester; chlorocarbonylbis(triphenylphosphine)rhodium(I); In water; N,N-dimethyl-formamide; at 140 ℃; for 0.25h; under 10343 Torr; microwave irradiation;

DOI:10.1016/j.tetlet.2003.10.032

Reference yield: 90.0%

para-bromotoluene (106-38-7) + hexanal (66-25-1) → pentyl 4-methylphenyl ketone (1669-33-6)

Guidance literature:

With pyrrolidine; 1,3-bis-(diphenylphosphino)propane; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 115 ℃; for 6h; Molecular sieve;

DOI:10.1021/ja804351z

Reference yield: 87.0%

1-(p-methylphenyl)cyclohexanol (1821-24-5) → pentyl 4-methylphenyl ketone (1669-33-6)

Guidance literature:

With 2,4,6-trimethyl-pyridine; iron(III) chloride; 1,2-bis(2,4,6-triisopropylphenyl)disulfane; tetrabutyl-ammonium chloride; In 1,2-dichloro-ethane; for 60h; Schlenk technique; Inert atmosphere; Irradiation; Sealed tube;

DOI:10.1021/acs.orglett.1c03137

upstream raw materials:

toluene

hexanoic acid

Hexanoyl chloride

n-hexanoic anhydride

Downstream raw materials:

2-morpholin-4-ylmethyl-1-p-tolyl-hexan-1-one

pentyl 4-methylbenzoate

p-Toluic acid

1-p-Tolyl-hexane-1,2-dione dioxime

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1669-33-6 1-p-tolylhexan-1-one

Send

Send

Metric Ton KG G Pound L ML

Send

Send