14-(p-chlorophenyl)-8-(p-chlorophenylsulphonylamino)-13-oxa-14-thia-1,15-diazapentacyclo<10.4.2.0^2,7.0^8,16.0^12,16>octadeca-2,4,6,14-tetraene S oxide

Base Information

• Chemical Name: 14-(p-chlorophenyl)-8-(p-chlorophenylsulphonylamino)-13-oxa-14-thia-1,15-diazapentacyclo<10.4.2.0^2,7.0^8,16.0^12,16>octadeca-2,4,6,14-tetraene S oxide
• CAS No.: 75319-68-5
• Molecular Formula: C₂₆H₂₃Cl₂N₃O₄S₂
• Molecular Weight: 576.524
• Mol file: 75319-68-5.mol

Synonyms:

Chemical Property of 14-(p-chlorophenyl)-8-(p-chlorophenylsulphonylamino)-13-oxa-14-thia-1,15-diazapentacyclo<10.4.2.0^2,7.0^8,16.0^12,16>octadeca-2,4,6,14-tetraene S oxide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 14-(p-chlorophenyl)-8-(p-chlorophenylsulphonylamino)-13-oxa-14-thia-1,15-diazapentacyclo<10.4.2.0^2,7.0^8,16.0^12,16>octadeca-2,4,6,14-tetraene S oxide

There total 2 articles about 14-(p-chlorophenyl)-8-(p-chlorophenylsulphonylamino)-13-oxa-14-thia-1,15-diazapentacyclo<10.4.2.0^2,7.0^8,16.0^12,16>octadeca-2,4,6,14-tetraene S oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-chlorobenzenesulfonyl azide (4547-68-6) + 1,2,2a,3,4,5-hexahydropyrrolo<3,2,1-jk>carbazole (74066-86-7) → 14-(p-chlorophenyl)-8-(p-chlorophenylsulphonylamino)-13-oxa-14-thia-1,15-diazapentacyclo<10.4.2.02,7.08,16.012,16>octadeca-2,4,6,14-tetraene S oxide (75319-68-5)

Guidance literature:

In tetrachloromethane;

DOI:10.1107/S0567740880007352

Reference yield:

p-chlorobenzenesulfonyl azide (4547-68-6) + 1,2,2a,3,4,5-hexahydropyrrolo<3,2,1-jk>carbazole (74066-86-7) → 12-(p-chlorophenylsulphnylamino)-6,7,10,11-tetrahydroazocino<1,2-α>indol-8(9H)-one (75319-67-4) + 3a-p-chlorophenylsulphonylamino-11-p-chlorophenylsulphonylimino-1,2,3,3a,4,5-hexahydro-11H-cyclopenta<2,3>pyrrolo<1,2-a>indole + 14-p-chlorophenyl-8-p-chlorophenylsulphonylamino-13-oxa-14-thia-1,15-diazapentacyclo<10.4.2.02,7.08,16.012,16>octadeca-2,4,6,14-tetraene S-oxide (75319-68-5) + 11-p-chlorophenylsulphonylimino-1,2,3,3a,4,5-hexahydro-11H-cyclopenta<2,3>pyrrolo<1,2-a>indole (76569-36-3)

Guidance literature:

In tetrachloromethane;

upstream raw materials:

p-chlorobenzenesulfonyl azide

1,2,2a,3,4,5-hexahydropyrrolo<3,2,1-jk>carbazole