Carbamic acid, [4-[[4-[[[(diphenylmethyl)amino]carbonyl]oxy]-1-piperidinyl]methyl]phenyl] methyl-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Carbamic acid, [4-[[4-[[[(diphenylmethyl)amino]carbonyl]oxy]-1-piperidinyl]methyl]phenyl] methyl-, 1,1-dimethylethyl ester
CAS No.:168830-88-4
Molecular Formula:C₃₂H₃₉N₃O₄
Molecular Weight:529.679
Hs Code.:
Mol file:168830-88-4.mol

Synonyms:

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Chemical Property of Carbamic acid, [4-[[4-[[[(diphenylmethyl)amino]carbonyl]oxy]-1-piperidinyl]methyl]phenyl] methyl-, 1,1-dimethylethyl ester

Chemical Property:

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Technology Process of Carbamic acid, [4-[[4-[[[(diphenylmethyl)amino]carbonyl]oxy]-1-piperidinyl]methyl]phenyl] methyl-, 1,1-dimethylethyl ester

There total 3 articles about Carbamic acid, [4-[[4-[[[(diphenylmethyl)amino]carbonyl]oxy]-1-piperidinyl]methyl]phenyl] methyl-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 168830-93-1
tert-butyl (4-(bromomethyl)phenyl)(methyl)carbamate

: 4-piperidyl benzhydrylcarbamate monohydrochloride

: 168830-88-4
[4-(4-benzhydrylcarbamoyloxy-piperidin-1-ylmethyl)-phenyl]-methyl-carbamic acid tert-butyl ester

Guidance literature:: With potassium carbonate; In acetonitrile; at 80 ℃;
DOI:10.1248/cpb.46.1274

Reference yield:

: 623-08-5
N-methyl-p-toluidine

: 168830-88-4
[4-(4-benzhydrylcarbamoyloxy-piperidin-1-ylmethyl)-phenyl]-methyl-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: CH₂Cl₂ / 24 h / Ambient temperature

2: N-bromosuccinimide, azobisisobuityronitrile / CCl₄ / 1 h / Heating

3: K₂CO₃ / acetonitrile / 80 °C

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); potassium carbonate; In tetrachloromethane; dichloromethane; acetonitrile;
DOI:10.1248/cpb.46.1274

Reference yield:

: 693803-44-0
tert-butyl N-p-tolyl-N-methylcarbamate

: 168830-88-4
[4-(4-benzhydrylcarbamoyloxy-piperidin-1-ylmethyl)-phenyl]-methyl-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: N-bromosuccinimide, azobisisobuityronitrile / CCl₄ / 1 h / Heating

2: K₂CO₃ / acetonitrile / 80 °C

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); potassium carbonate; In tetrachloromethane; acetonitrile;
DOI:10.1248/cpb.46.1274