9(10H)-Anthracenone, 10,10-bis(4-hydroxyphenyl)-

Base Information

• Chemical Name: 9(10H)-Anthracenone, 10,10-bis(4-hydroxyphenyl)-
• CAS No.: 16889-49-9
• Molecular Formula: C26H18O3
• Molecular Weight: 378.427
• Mol file: 16889-49-9.mol

Synonyms:10,10-Bis-(4-hydroxy-phenyl)-anthron;10,10-bis(4-hydroxyphenyl)anthrone;10,10 bis-(4-hydroxyl phenyl) anthrone;10,10-bis-(4-hydroxy-phenyl)-anthrone;9,9-Bis(4-hydroxyphenyl)-10-anthron;9,9'-bis(4-hydroxyphenyl)anthrone-10;

Chemical Property of 9(10H)-Anthracenone, 10,10-bis(4-hydroxyphenyl)-

Chemical Property:

• PSA: 57.53000
• LogP: 5.02490

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 9(10H)-Anthracenone, 10,10-bis(4-hydroxyphenyl)-

There total 6 articles about 9(10H)-Anthracenone, 10,10-bis(4-hydroxyphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.58%

9,10-phenanthrenequinone (84-65-1) + phenol (108-95-2,27073-41-2) → 9,9'-bis(4-hydroxyphenyl)-10-anthrone (16889-49-9)

Guidance literature:

With methanesulfonic acid; 3-mercaptopropionic acid; In 1,2-dichloro-ethane; at 60 - 65 ℃; for 4h;

Reference yield:

9-acetoxy-10-(4'-acetoxyphenyl)-anthracene (57374-14-8) → 9,9'-bis(4-hydroxyphenyl)-10-anthrone (16889-49-9)

Guidance literature:

Multi-step reaction with 3 steps

1: acetic acid; aqueous Na₂Cr₂O₇

2: aq.-ethanolic NaOH

3: sulfuric acid

With sodium hydroxide; sodium dichromate; sulfuric acid; acetic acid;

DOI:10.1021/ja01868a084

Reference yield:

10-hydroxy-10-(4'-acetoxypheny)-anthrone-9 (85773-93-9) → 9,9'-bis(4-hydroxyphenyl)-10-anthrone (16889-49-9)

Guidance literature:

Multi-step reaction with 2 steps

1: aq.-ethanolic NaOH

2: sulfuric acid

With sodium hydroxide; sulfuric acid;

DOI:10.1021/ja01868a084

upstream raw materials:

9,10-phenanthrenequinone

phenol

10-hydroxy-10-(4'-hydroxyphenyl)anthrone-9

9-acetoxy-10-(4'-acetoxyphenyl)-anthracene

Downstream raw materials:

9,10-phenanthrenequinone

phenol

10,10-bis(4-methoxyphenyl)(10H)anthracen-9-one

10-Hydroxy-9.9.10-tris-(4-methoxy-phenyl)-9.10-dihydro-anthracen