3,10-Perylenedione,4,9-dihydroxy-1,12-bis[(2S)-2-hydroxypropyl]-2,6,7,11-tetramethoxy-, (6aR)-(9CI)

Base Information

• Chemical Name: 3,10-Perylenedione,4,9-dihydroxy-1,12-bis[(2S)-2-hydroxypropyl]-2,6,7,11-tetramethoxy-, (6aR)-(9CI)
• CAS No.: 77115-15-2
• Molecular Formula: C₃₀H₃₀O₁₀
• Molecular Weight: 550.562

Synonyms:3,10-Perylenedione,4,9-dihydroxy-1,12-bis(2-hydroxypropyl)-2,6,7,11-tetramethoxy-, stereoisomer;(+)-Calphostin D; Isophleichrome; iso-Phleichrome

Chemical Property of 3,10-Perylenedione,4,9-dihydroxy-1,12-bis[(2S)-2-hydroxypropyl]-2,6,7,11-tetramethoxy-, (6aR)-(9CI)

Chemical Property:

Purity/Quality:

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Technology Process of 3,10-Perylenedione,4,9-dihydroxy-1,12-bis[(2S)-2-hydroxypropyl]-2,6,7,11-tetramethoxy-, (6aR)-(9CI)

There total 52 articles about 3,10-Perylenedione,4,9-dihydroxy-1,12-bis[(2S)-2-hydroxypropyl]-2,6,7,11-tetramethoxy-, (6aR)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1,12-Bis-((S)-2-hydroxy-propyl)-2,6,7,11-tetramethoxy-4,9-bis-methoxymethoxy-perylene-3,10-dione (133379-36-9) → phleichrome (56974-44-8,77115-15-2,124986-26-1,125411-34-9,127180-30-7,132880-98-9,136374-42-0)

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; methanol; water; at 20 ℃; for 0.0333333h;

DOI:10.1016/S0040-4039(00)92105-1

Reference yield:

C32H34O10 → isophleichrome (56974-44-8,77115-15-2,124986-26-1,125411-34-9,127180-30-7,132880-98-9,136374-42-0)

Guidance literature:

With magnesium iodide; In tetrahydrofuran; diethyl ether; for 0.166667h; Inert atmosphere;

DOI:10.1021/ja902324j

Reference yield:

1,12-Bis-((S)-2-hydroxy-propyl)-2,6,7,11-tetramethoxy-4,9-bis-methoxymethoxy-perylene-3,10-dione (133379-36-9) → isophleichrome (56974-44-8,77115-15-2,124986-26-1,125411-34-9,127180-30-7,132880-98-9,136374-42-0)

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; methanol; water; at 20 ℃; for 0.0333333h;

DOI:10.1016/S0040-4039(00)92105-1

upstream raw materials:

phleichrome

1,12-Bis-((S)-2-hydroxy-propyl)-2,6,7,11-tetramethoxy-4,9-bis-methoxymethoxy-perylene-3,10-dione

2-bromo-1,5-dimethoxy-3-methylbenzene

2,4-dimethoxy-6-methylbenzoic acid

Downstream raw materials:

isophleichrome

hypocrellin-B

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