1,3-dimethoxy-2-propylbenzene

Base Information

• Chemical Name: 1,3-dimethoxy-2-propylbenzene
• CAS No.: 16929-64-9
• Molecular Formula: C11H16O2
• Molecular Weight: 180.247
• Hs Code.: 2909309090
• Mol file: 16929-64-9.mol

Synonyms:1,3-dimethoxy-2-propyl-benzene;Benzene,1,3-dimethoxy-2-propyl;2,4,Dimethoxy-3-propylbenzene;2-Propyl-1,3-dimethoxybenzene;

Chemical Property of 1,3-dimethoxy-2-propylbenzene

Chemical Property:

• Vapor Pressure: 0.0563mmHg at 25°C
• Boiling Point: 241.2oC at 760 mmHg
• Flash Point: 83.3oC
• PSA: 18.46000
• Density: 0.965g/cm3
• LogP: 2.65630
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

1,3-Dimethoxy-2-propylbenzene 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,3-dimethoxy-2-propylbenzene

There total 2 articles about 1,3-dimethoxy-2-propylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

1-iodo-propane (107-08-4) + 1,3-Dimethoxybenzene (151-10-0) → 1,3-Dimethoxy-2-(prop-1'-yl)benzene (16929-64-9)

Guidance literature:

1,3-Dimethoxybenzene; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃; for 2h;

1-iodo-propane; In tetrahydrofuran; hexane; at 0 - 20 ℃;

DOI:10.1016/j.bmcl.2015.01.047

Reference yield:

→ 1,3-Dimethoxy-2-(prop-1'-yl)benzene (16929-64-9)

Guidance literature:

1,3-Dimethoxybenzol, 1. PhLi (Ether), 2. Propyliodid (Toluol, 5h, Kochen);

Reference yield: 96.0%

1,3-Dimethoxy-2-(prop-1'-yl)benzene (16929-64-9) → 2,4-dimethoxy-3-propylbromobenzene (118684-06-3)

Guidance literature:

With N-Bromosuccinimide; In N,N-dimethyl-formamide; for 48h; Ambient temperature;

upstream raw materials:

1-iodo-propane

1,3-Dimethoxybenzene

Downstream raw materials:

2-propyl-1,3-benzenediol

2,4-dimethoxy-3-propylbromobenzene

3-methoxy-2-propylphenol

3-(2-cyanophenoxy)2-propylphenol

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